Volumetric analysis 1:
https://www.creative-chemistry.org.uk/documents/N-ch1-35.pdf
Volumetric analysis 2 :
https://www.creative-chemistry.org.uk/documents/N-ch1-36.pdf
Volumetric Analysis A level part 1 : Making standard solution of sodium carbonate
Hazcard : 95A
Goggles
Bench mat
pens
Balances 0.1g (main prep) X 2
Balances 0.01g (use all 7 from Chem prep)
100 cm3 beaker
250 cm3 beaker
250 cm3 volumetric flask with stopper
Filter funnel
Glass rod
Teat pipette
Spatula
Label De-ionised water
Anhydrous sodium carbonate, Na2CO3(s) (in 125cc beaker place in blue tray between balances minimum 3g)
Volumetric Analysis A level part 2 : To standardise Hydrochloric acid
Hazcard : 95A, 47A, 32,
Goggles
100 cm3 beaker
250 cm3 beaker
250 cm3 conical flask (Titration kit)
25 cm3 bulb pipette (titration kit)
Pipette filler (titration kit)
Burette and Burette stand and holder (titration kit)
Plastic filter funnel (titration kit)
White tile (titration kit)
Teat pipette
Distilled water
Access to :
standard sodium carbonate solution (Made up in Part 1)
dilute hydrochloric acid to standardise 0.075 M (2.5L) labelled HCl (no molarity)
phenolphthalein indicator solution
methyl orange indicator solution
From 2M HCl : Final volume X New Molarity / Original Molarity
2500ml X 0.075M /2M = 94Ml of 2M in 2406 water using Standard flask((Volumetric)Very Accurate), Fill up the large 2L Standard flask with water , pour 94Ml of 2M HCl to up to 2.L then pour in 2.5l bottle. Then using 500Ml volumetric flask rinse and top up to 2.5l. shake new acid bottle.
Clean Volumetric with water and rinse with distill water.
2.5 litre bottle of HCl and more on the side in case instead of stock bottle
Volumetric Analysis A level part 3 :
Hazcard :
Class set :
Analytical balances
Distilled water wash bottle
Hydrochloric acid 0.10 M (about 200 cc per student)
(Check if labeling require Strength of HCl visible or not)
Sodium carbonate Solution
Sodium carbonate Solid (about 2.5 g per student)
Methyl orange indicator
Per Student :
Safety google
2 X 100 cc beaker
2 X 250 cc beaker
2 X conical flask (titration)
1 X Glass funnel (titration)
1 X Glass rod
250 cc Volumetric flask and stopper
25 cc bulb pipette (titration)
1 X pipette filler
1 X burette (titration) and Stand
Weighing bottle/boat
1 X spatula
White tile (titration)
1 X small plastic funnel
1 X copy of N-chl-37 (Student guide practical)