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Pract. 34 Exp. C 2 Reaction with Nitrous acid HAZCARD : 2A,93, 3A,70A,91A, 70B, 47A
Spatula
Ammonium chloride
Kettle
Tripod, gauze, Benson burner, HPM
Test tubes
Beaker
Teat pipettes
Solid sodium nitrITE cupboard1 ***
Con. HCl
Butylamine Display in fume
Dilute HCl 1Mol
Phenylamine (aniline) cupboard 1 display in fume
Crushed Ice
Phenol solid cupboard1 display in Fume
Dilute NaOh 1 mol.
2-naphthol
Gloves
Distilled water
2 X tray of Crushed ice
Large beaker for Waste Organic !!
***Near miss : Careful to sodium NITRATE(cupboard2) and NITRITE (Cupboard1)
Conc HCL in fume
Waste AZo Dyes fume cab. N-Butylamine fume cab Phenylamine fume cab. Phenol cristal fume cab.
A 1: Reaction of amines as bases
Butylamine Display in fume
Phenylamine (aniline) cupboard 1 display in fume
Distilled water
UI paper
Ammonia solution
Test tubes bungs
teat pipette
A 2 : Reaction with dilute HCl
Butylamine Display in fume
Phenylamine (aniline) cupboard 1 display in fum
Dilute HCl
Dilute sodium hydroxide
Test tubes bungs and rack
Teat pipettes
Gloves
Large beaker for Waste Organic !!
B : Reactions of amine as ligands
Ammonia solution (A level)
Copper(II) sulphate solution (about 0.1 M)
Butylamine Display in fume
Phenylamine (aniline) cupboard 1 display in fum
Ammonia solution
Test tubes and bungs and rack
Teat pipettes
Gloves
Large beaker for Waste Organic !!
C : Reaction of amines as nucleophiles
1 Reaction with erthanoyl chloride and benzoyl chloride
Phenylamine (aniline) cupboard 1 display in fume
Boiling tubes bungs and rack
Teat pipettes
ethanoyl chloride (Acetyl chloride)
Gloves
Large beaker for Waste Organic !!
D : Reaction of the aromatic ring in Phenylamine
Phenylamine (aniline) cupboard 1 display in fum
Test tubes
HCl Conc.
Teat pipettes
Bromine water
Large beaker for Waste Organic !!
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