17.5 Preparation of Cyclohexene GAS ON HAZCARD :
Per set
5cc of 85% phosphoric acid
10cc of Cyclohexanol
50cc pear shape flask (Quick fix)
tripod and gauze (In Class)
quick fix condenser for re-flux, quick fix holder
quick fix still head, thermometer holder, receiver bend for distillation
2 X small conical flask (Main Prop.)
Thermometer (In Class)
anti-bumping granules (Chem Prep.)
Separating funnel (Quick fix)
Distilled water (Chem prep.)
150ml large beaker (Clean container) (In Class)
Spatula (Chem pre.)
Anhydrous calcium chloride
cotton wool or filter paper (In Class- Chem prep.)
sample tube (Chem prep.)
Balances (Chem prep.)
Vaseline
stopper for separating funnel delivery bend, still head, thermometers holder liebig condensors 7B5
Pear shape flask separating funnel