DEPT
DEPT Expt - ACQU
1. After 13C experiment , take the DEPT expts directly without atmm again.
(測完 13C 後再連續測dept, 就不需要atmm)
DEPT90 : Acqu
2. edc (create a new expno)
(設新的expno , expno為置放實驗fid處, procno為置放數據處理區)
(Note: expno for fid raw data, procno for processing data)
3. rpar bbfo_13C_dept90 (read in the parameter set of expt, eg: acqu,proc,plot,title etc)
4. getprosol (get the correct pulse width and power lever with the current probehead)
5. ns 256 (ns = 8~1024) It depends on concentration.
6. rga (receiver gain auto adjust)
7. zg
DEPT135 : Acqu
8. edc (create another new expt)
9. rpar bbfo_13C_dept135
10. getprosol
11. rga
12. ns 256 (ns = 8 ~ 1024)
13. zg (zero and go)
* use halt to terminate the acquisition.
* use tr for data transfer to temporary area without interrupting acquisition.
* use efp to (em)exponential multiplication and (ft) fourier transformation
and (pk)phase correction.