Bruker AVIII 400MHz NMR 管理辦法- B662
Draft Amendments to the Operating and Management Regulations for NTU Department of Chemistry's Bruker AVIII 400 NMR - B662
I. Examination Rules Explanation
All users must pass an examination to obtain operational and access permissions before independently operating the instrument. Operation is not allowed without passing the examination.
Those seeking operational permission must have a thorough understanding of the operation methods and steps before taking the exam. Practical hands-on training, supervised by management personnel or certified individuals, is required at least twice.
Practice sessions are limited to 30 minutes per person, per session, and must be scheduled with management personnel or individuals with operational permissions.
Users eligible for training and examination include:
Researchers engaged in relevant research within the department with the consent of their supervising professor.
Limited to users related to the department.
Examination Schedule:
Examinees must arrange the examination time with management personnel.
Examination Principles:
Management personnel are responsible for preparing test samples, primarily using known samples.
Examinees must independently complete the data collection and processing of proton and carbon spectra (including DEPT series experiments) within the specified time, with management personnel present.
Management personnel may suspend the exam based on the situation. Those who do not pass the exam must practice twice before reapplying.
In case of incorrect operations leading to equipment damage during the exam, the laboratory to which the user belongs will collectively share the repair costs.
Other advanced experiments, such as variable temperature and 2D experiments, require discussion with management personnel and acceptance of relevant training and tests before operation. Otherwise, in the event of equipment damage, the laboratory to which the user belongs will share the repair costs (the instrument board is expensive, each worth at least tens of thousands of dollars).
II. Open Rules Explanation
Users with operational permission must use their own access cards and accounts.
Users must record their start and end times in the usage logbook, and can leave only after completing the log and usage details (failure to do so will result in all relevant data being sent to the respective teachers).
Sharing access cards, accounts, and passwords with others is strictly prohibited. If discovered, the first offense will result in a warning and an email notification to the supervising professor. The second offense will result in a one-month suspension of NMR usage.
Management personnel and responsible teachers may inspect usage at any time.
When users cause equipment damage due to non-compliance with instructions, the laboratory to which the user belongs must collectively share the repair costs.
A. Instrument Availability
Instrument availability is divided into half-hour laboratory rotations during the day and long-term individual rotations.
AVIII 400 NMR (B662) is available for laboratory rotations from 1:00 pm to 10:00 pm.
Fridays from 9:30 am to 11:30 am are reserved for instrument calibration and liquid nitrogen filling, suspending open usage.
For maintenance, repair, or experimental testing of other instruments, management personnel may announce temporary suspension of instrument usage.
(1) [Segment A - From 8:00 AM to 10:00 AM, a total of 2 hours]
[Segment B - From 10:00 AM to 1:00 PM, a total of 3 hours]
(2) Those who sign up for Segment B have the first priority to renew Segment A (reservation rotations count as one time).
(3) Those who sign up for the long-term rotation on the previous night have the second priority to renew Segment A (reservation rotations count as one time).
(4) Each person is allowed one rotation per week. Those with additional needs must wait for the evening rotations on the previous day, the current day, or Friday evening. The drawing of lots or application submission will determine the assignments during these rotations.
B. Laboratory Rotation Time Reservation
The reservation of instrument usage is organized by laboratory units. Users from each laboratory take turns signing up for time slots according to the order listed in the NMR room rotation schedule.
Only one time slot (30 minutes) can be signed up for at a time. If the first priority user does not arrive, the second priority user fills the slot.
After the first priority user signs up, the next user in the rotation schedule signs up. This continues until no one is left or until all regular usage time slots are filled.
The first priority user today becomes the last priority user tomorrow, and the second priority user today becomes the first priority user tomorrow.
If time slots are still available after the first round, a second round of sign-ups is opened. (No third round is available.) Users are encouraged to coordinate and start signing up from the beginning of each hour during the first round.
Users who are not punctual forfeit their turn.
Representatives must come to reserve rotation time slots at the designated times in the afternoon (5:30 PM for room A525 on the fifth floor and 5:35 PM for room B662 on the sixth floor). In case of holidays, reservations are made on the day before the holiday. For example, on weekends, reservations can be made on Friday evening for Saturday, Sunday, and Monday usage.
Reserved time slot users must start operating the equipment promptly at the reserved time. If they are more than two minutes late, they lose their priority usage rights, and the next person in line takes their turn.
C. Personal Long-Term Rotation Reservation
AVIII 400NMR (B662) long-term rotations have two time periods:
morning (8:00 AM - 1:00 PM) and overnight (10:00 PM - 8:00 AM the next day).
Rotation occurs once a week, and users self-designate time slots on Monday evenings at 5:35 PM (B662). Users must specify their research group, Chinese name, and laboratory phone number when signing up.
Fourteen time slots are open for rotation each week, starting from Tuesday and ending on the following Monday.
Users can only select one time slot per week, except on Sundays, where they can choose two time slots. Users must choose either weekday or Sunday slots, not both. The chosen time slots are considered claimed, regardless of actual usage (as it is based on individual users, not laboratories). The frequency of rotation sign-ups may be adjusted based on circumstances.
Users needing long-term usage must come in person or send a designated representative to reserve a time slot.
Order of reservation is determined by drawing lots or coordination.
Unfilled time slots are given to users on a first-come, first-served basis. In the case of simultaneous arrivals, drawing lots or coordination will decide. Long-term users should indicate their status on the long-term usage schedule.
Users who don't need a time slot should refrain from randomly filling out the schedule. Filling out a time slot for long-term experiments is considered claiming that time and incurring charges, regardless of actual usage. Administrators will use timing software to check for actual usage, and if no records are found, fees may be pursued (unit price x hours x n, where n > 2).
Except for the Monday evening rotation sign-up, if there are still vacant time slots later in the week, they can be assigned on the previous day or the same day in the evening. For weekend time slots (Saturday to Monday), assignments can be made on Friday evening.
Those who reserve a time slot but cannot come for long-term usage must cancel no later than the rotation sign-up time.
Emergency applications for special needs will be considered and assisted.
D. Service Types and Fee Standards
The instrument does not provide testing services but offers educational training and consultation services.
Relevant educational training will be offered as needed each academic year.
The instrument operation fee is charged on a per-laboratory basis.
Each NMR account (regardless of the number of devices) will be charged an annual account setup fee per laboratory.
The NMR room will provide written guidance on basic experimental procedures and precautions.
E. Notes and Management Rules
Notes:
The instrument room is equipped with two surveillance systems, and there are access control and surveillance systems outside the instrument room. Passwords are provided based on need and without compromising the security of the surveillance system.
USB drives are not allowed inside the instrument room, and users are not allowed to install software on the computer arbitrarily.
Each professor's laboratory uses an independent account and password. (Independent accounts are used to protect the files of individual laboratories.)
The instrument cannot initiate NMR operations without an account and password.
If a user's account has not ended, the next account cannot execute experiments. Users must remember to log out of their accounts after experiments.
If needed, an administrator may stop tasks being executed by an account in emergency situations, potentially resulting in data loss.
Long-term experimenters should pay attention to the experiment setup and accurately estimate the required time for the experiment, making it convenient for them to come and finish the experiment on time or earlier the next day. Remember: complete the log-out action when the experiment ends to facilitate the next account's usage. Do not log out if the experiment is not finished, as it will be terminated.
Experiment data processing should be done on the Process PC or the laboratory's PC.
Under normal circumstances, account passwords can be applied for and changed annually.
The NMR room does not provide a printer to save machine time.
Eating is not allowed in the NMR room, and personal items must be taken away when leaving.
The instrument automatically records the user's login time, which is the basis for instrument operation charges. Users must remember to log out of their accounts after experiments. Do not lend your account or password to others, as this affects the interests of each laboratory.
Violations List:
Intentional destruction of computers or networks.
Failure to notify management when an NMR TUBE breaks inside the instrument probe.
Deliberately terminating experiments on original samples during someone else's scheduled time, replacing them with personal samples, and then returning the original samples after testing. (This situation will be investigated by reviewing the login events on the computer and checking surveillance footage in case of abnormal experiments.)
Leading individuals from other departments or external individuals to operate NMR without permission.
Operating without a license, without the accompaniment of a supervisor (Ph.D. or M.Sc.), or using someone else's card without permission.
Leaving without signing the logbook.
Conducting experiments without following management rules. (Any violations will be reported to the responsible NMR professor and the supervisor of the person involved, or sent to the department for disciplinary actions, including suspension.)
F. File Management:
Each laboratory will use an independent account named after the teacher, and laboratory members will create their own subdirectories under the same account.
Each account will be allocated 2 GB of storage space for file storage.
Each laboratory is responsible for managing files, deciding whether to keep, delete, or back up files. Once the storage limit of 2 GB is exceeded, no further files can be saved, and no more experiments can be conducted.
If management personnel need to clear all files for an account belonging to the same laboratory, they must obtain consent from the supervisor, who will assist in completely deleting all files for that account.
It is recommended to name files using the format "Name-YYYYMMDD-SampleNumber" to facilitate future file searches.
(G) Bruker AVIII 400NMR (B662) Daytime Reservation Rotation Order Table
ChanCC (陳振中) -> ChanYT(詹益慈) -> ChenCT (陳昭岑) -> ChenHM (陳浩銘) ->
ChenRP (陳 平) -> ChiuCW (邱靜雯) -> ChiuSH (邱勝賢) -> ChouPT (周必泰) ->
ChuJ (朱忠瀚) -> Farrell (方頡睿) -> KongKV (江建文) -> LeungMK (梁文傑) ->
LiaoWS (廖尉斯) -> LiuST (劉緒宗) -> LoLC (羅禮強) -> MouCY (牟中原) ->
PengCH(彭之皓) -> WangTS (王宗興) ->WongKT (汪根欉) -> YangJS (楊吉水) ->
YooWJ (柳玗珍)
1) The order is based on the alphabetical order of the professors' last names.
2) The daytime order must be rotated daily (only those who are not late have the possibility of signing up for a time slot).
3) Laboratories not on the daytime order table can apply if needed
國立台灣大學化學系Bruker AVIII 400 NMR使用及管理辦法草案修正 - B662
一、考試規則說明
1. 所有使用者均需通過考試取得操作與門禁許可方可獨立操作，在未通過考試前不得獨自操作儀器。
2. 欲取得操作許可者在參加考試前需確實了解操作方法與步驟，且上機實際練習兩次以上(需有管理人員或已取得認證者在現場指導) 。
3. 練習時間每人每次以30分鐘(由管理人員或有操作許可者預約時段)為原則。
可參與訓練及考試之使用人員 :
1. 本系從事相關研究者，經指導教授同意者。
2. 僅限本系相關使用者
考試時間 :
考生請與管理人員約定考試時間。
考試原則 :
1. 管理人員負責準備測試樣品，原則上以已知樣品為主。
2. 考生須於指定時間內，於管理人員在場時，自行完成氫譜與碳譜(含DEPT系列實驗)數據之採集與處理。
3. 管理人員得視情況中止考試，未通過考試者需再上機練習二次始得申請參加考試。
4. 考試過程中若不正確之操作而導致設備損壞時，由該員所屬之實驗室共同分擔維修費用。
5. 其它進階實驗的操作，如變溫與2D實驗等，須另與管理人員討論並接受相關訓練與測驗，始得操作。如否，設備損壞時將由該員所屬
之實驗室共同分擔維修費用。(儀器板子很貴，每片值至少數拾萬元)
二、開放規則說明
1. 具操作許可之使用者需使用自己之門卡與帳號
2. 使用者須先在使用記錄簿上填寫起始使用時間，使用完畢後登錄簽退時間，填寫使用狀況後始得離去(沒有填寫者，將以畫面傳送
所有相關老師認領)
3. 嚴禁將門卡與帳號及密碼交予他人使用，如經發現，借卡或被借卡者，首次先予以警告並E-Mail通知指導教授，第二次將暫停使用
NMR一個月
4. 管理人員及負責老師得隨時抽查使用狀況
5. 當使用者未照指示操作而導致設備損壞時，該人員所屬之實驗室需共同分擔維修費用。
A. 儀器開放
1. 儀器開放分為日間1/2小時實驗室輪簽及長時間個人輪簽
2. AVIII 400 NMR(B662)自下午一點起至晚上十點為實驗室輪簽。
3. 星期五上午9:30am 至11:30am為預定儀器校正與液氮充填時段，暫停開放使用
4. 其它儀器維護及修理或實驗測試所需時間，管理人員得公佈儀器暫停使用
(1)【A段–自8:00AM 至 10:00AM 共 2小時】
【B段–自10:00AM 至 13:00PM 共 3小時】
(2)簽 B 段者 有第一優先權去續簽 A 段(預約輪簽合算1 次)
(3)簽前一天夜晚之長時間者 有第二優先權去續簽 A 段(預約輪簽合算1 次)
(4)每人一星期輪簽只有一次，有更多需要者需待 前一天/當天/星期五 傍晚輪簽時抽簽劃定或提出申請
B. 實驗室輪簽時間預約
1. 儀器之預約使用時段，以實驗室為單位，
按照NMR室所列之順序表由到場之各實驗室值簽人員輪流簽定。
2. 一次只可簽一個時段(30分鐘)，若第一順位未到則由第二順位遞補簽定。
3. 第一順位簽完後由輪值表下一順位簽，如此輪流到無人要簽或一般使用時段簽完為止。
4. 今天的第一順位者為明天最後順位，今天第二順位者為明天第一順位。
5. 若第一輪簽完尚有時段，開放第二輪輪簽。(沒有開放第三輪)
(若是能夠請自行協調，第一輪從整點開始簽)
6. 沒有準時到場者，當棄權論。
7. 每日下午於指定時間 (五樓A525室為5:30PM及六樓B662室為5:35PM) 派代表來預約輪簽時段。
遇假日則以假日前一天預約為原則，
例如週六，日為週休日則週五晚上可以預約週六、週日及週一之使用時段。
8. 預約時段者應依預約時間準時上機操作，逾時二分鐘，即喪失該時段之優先使用權，並由現場等候者依序上機。
C. 個人長時間輪簽預約
1. AVIII 400NMR(B662)長時間輪簽有每日上午及夜間2種時段
2. 上午時段8:00AM -1:00PM，夜間時段10:00PM- 8:00AM(隔日)。
3. 每星期輪簽一次，於星期一傍晚5:35PM(B662)由使用者自行劃定時段。
輪簽者需要註明研究群、使用者之中文姓名以及實驗室電話號碼。
4. 每一次開放一星期之時段(14個段落)供輪簽，自星期二開始到下星期一。
5. 每一使用者週間時段一次只能選一時段，週日可選二時段。
週間時段與週日時段二者只能擇一。
填寫之時段等於認領時段時間及費用(不論有沒有來測)。
( 因為是以使用者個人非以實驗室，故暫時開放輪簽一次，將視情況調整。)
6. 有需要長時間之使用者需要本人或指定代表來預約。
7. 填寫順序由擲籤或協調決定
8. 沒有被填滿之時段，使用者先到先測。
同時到者，由擲籤或協調決定。
惟來測者若屬於長時間使用請在長時間使用表註記。
9. 沒有需要者，請勿任意填寫。
長時間實驗之填寫時段等於認領那個時段時間及費用，
管理員會用計時程式抽查有無實際使用，若
無實際記錄，將視情況追討其費用(即單價x時數x n)。n>2
10. AVIII 400長時間輪簽除在星期一傍晚輪簽時抽簽劃定外，
若當週尚有空白時段；可在前一天或當天傍晚輪簽時抽簽劃定，
週末部份空白時段(星期六至星期一)可在星期五劃定。
前一天或當天傍晚預約者沒有限制是否當週預約過。
(換句話說，星期一傍晚沒有去簽長時間的話，
在本週開放的額度內，隨時可以登記一個時段，
若已登記者還有需要，需等待前一天或當天傍晚的輪簽時間才能再去簽定。)
11. 預約者無法前來使用長時間時段者，請務必最晚於輪簽前取消
12. 有特殊需要的可提出緊急申請，會協助安排
D. 服務類別與收費標準
1. 儀器原則上不提供代測服務，但是提供教育訓練及諮詢服務。
2. 每學年將視情況需要開辦相關教育訓練。
3. 儀器操作收費標準以實驗室為單位
4. 每一NMR帳號(不論設幾台)將以實驗室為單位，每年收取帳號設定費
5. NMR室將提供書面資料之基本實驗之實驗步驟指引及注意事項。
E. 注意事項及管理規則
注意事項
1. 儀器室內配有二套監視系統，儀器室外有門禁系統及監視系統，將視需要及不影響監視系統之安全之情況下開放密碼。
2. 儀器室內不得使用隨身碟，且不得任意於電腦安裝軟體。
3. 各教授實驗室使用一獨立帳號及密碼。
(獨立帳號是為了保護個別實驗室之檔案)
4. 此儀器沒有帳號密碼無法啟動NMR作業程式。
5. 此儀器在前帳號未結束前，下個帳號無法執行實驗。
使用者在實驗結束後一定要記得登出帳號。
6. 儀器若在不得已情況下需要由管理人員停止帳號正在執行之任務，
因而造成實驗數據可能無法保住。
7. 長時間實驗者請注意實驗之設定方式和仔細核算實驗所須時間，
方便隔日自己準時或提早前來結束 實驗並登出帳號。
記住:實驗結束時一定要完成登出動作，方便下一個帳號使用。
實驗尚未結束時，就不要登出，否則實驗將中止。
8. 實驗數據之處理在Process PC 或實驗室之PC上處理
9. 正常情況下，帳號密碼每年提供統一申請及更換。
10. NMR室不提供印表機，以節省佔機時間。
11. 不得在NMR室飲食，個人之物品請務必於離開時一併帶走。
12. 此儀器會自動統計使用者登入之佔機時間，為儀器操作收費之標準。
使用者在實驗結束後一定要記得登出帳號，
亦請勿任意出借帳號或密碼予他人；
因此事攸關各實驗室之權益。
違規行為表列
1. 蓄意破壞電腦或網路者。
2. NMR TUBE破裂於儀器探頭內而未通知管理人員者。
3. 在不屬於自己的時段，刻意終止原樣品之實驗進行，
置入自己之樣品取代原樣品，測試後再置入原樣品者。
(此情況將於實驗異常時，將電腦帳號登入事件檢視時程及調閱監視錄影帶作比對處置)
4. 在未經同意前，自行帶領外校系、或校外人士操作使用NMR者。
5. 在未取得執照前，沒有管理人員或學長之(博班或碩班)陪同操作，或借他人卡來使用者。
6. 未簽log book而離去者。
7. 不遵守管理規則隨意進行實驗者。
(若有違規行為，將視情節之輕重呈送NMR負責教授及該員所屬指導教授或送系所裁示懲處方式-包含停權處分)。
F. 檔案管理
1. 各實驗室將以老師名字使用獨立帳號，
實驗室成員在同一帳號下用自己之子目錄來建檔。
2. 各帳號將分配到2G大小之部分硬碟供儲存檔案。
3. 各實驗室需要自行管理檔案，或保留或刪除或另行備份，
由實驗室檔案使用者自行決定，惟超過2G後就無法再儲存任何檔案或進行任何實驗。
4. 若須管理人員清除所屬帳號同一實驗室所有成員之檔案，
須取得指導教授同意書，將協助全面刪除此帳號之所有檔案。
5. 建議檔案命名方式，儘量以「姓名-年年月月日日-樣號」之型式儲存檔案，
此格式對於日後尋找檔案非常有助益。
(G)Bruker AVIII 400NMR (B662) 實驗室日間預約輪簽順序表
ChanCC (陳振中) -> ChanYT(詹益慈) -> ChenCT (陳昭岑) -> ChenHM (陳浩銘) ->
ChenRP (陳 平) -> ChiuCW (邱靜雯) -> ChiuSH (邱勝賢) -> ChouPT (周必泰) ->
ChuJ (朱忠瀚) -> Farrell (方頡睿) -> KongKV (江建文) -> LeungMK (梁文傑) ->
LiaoWS (廖尉斯) -> LiuST (劉緒宗) -> LoLC (羅禮強) -> MouCY (牟中原) ->
PengCH(彭之皓) -> WangTS (王宗興) ->WongKT (汪根欉) -> YangJS (楊吉水) ->
YooWJ (柳玗珍)
1)排序表是依據各位實驗室負責教授其姓氏之英文字母排列
2)日間順序表需每天輪簽(不遲到者才有可能簽到時段)
3)沒有在日間順序表的實驗室若有需求可以提出申請