Shimadzu ICP-MS 2030LF Inductively Coupled Plasma Mass Spectrometer

Shimadzu ICP-MS 2030LF Inductively Coupled Plasma Mass Spectrometer (CCRL21)

Located in room 2202 of the Science Center Building of the Armstrong Campus.

The Shimadzu ICP-MS 2030LF, integrated with the Teledyne ASX-280 autosampler, is a high-performance system for the automated, sensitive, and cost-effective analysis of trace elements in various liquid samples. The combined system streamlines lab workflows by automating sample introduction, reducing manual error, and increasing sample throughput. 

Shimadzu ICP-MS 2030LF capabilities:

The Shimadzu ICP-MS 2030 offers sensitive trace-level and ultra-trace-level elemental analysis, as well as simultaneous measurement of major components. The system features proprietary technologies and intelligent software for simplified operation and low running costs. 

Performance:

• High sensitivity: A newly developed collision cell and optimized internal ion path geometry achieve superior sensitivity by efficiently removing molecular and polyatomic ions using only helium gas.

• Wide dynamic range: A secondary electron multiplier allows for a nine-order-of-magnitude dynamic range, enabling the simultaneous analysis of both major and trace-level components.

• Reduced interference: In addition to the collision cell, the system uses "On-Line Inter-Element Correction (IEC)" to automatically correct for spectral interference that is not eliminated by the cell. 

Cost-efficiency:

• Low gas consumption: A proprietary "Mini-Torch" plasma system reduces argon gas consumption by two-thirds compared to conventional torches.

• "Eco Mode": During standby, an "Eco Mode" minimizes gas flow and power consumption, further reducing operating costs.

• Lower-purity argon: The system can operate on more affordable 99.95% purity argon gas, unlike conventional systems that require higher-purity gas. 

Operational efficiency:

• • • • Analysis assistant functions: The software includes a "Development Assistant" for automatic method development and a "Diagnosis Assistant" for post-run interference checking.

      • Easy maintenance: An easy-to-maintain sample injection system and tool-free access to the torch and interface unit minimize downtime.

      • Software compliance: The LabSolutions ICPMS software supports network integration and complies with regulations like FDA 21 CFR Part 11. 

      • Teledyne ASX-280 autosampler features

      • The ASX-280 is a compact, robust autosampler that automates the liquid sample introduction process, improving throughput and reliability. 

Design and functionality:

• • • • Compact size: A small footprint helps to preserve laboratory bench space.

      • High throughput: The system can hold up to 180 samples, automating the workflow for low-to-medium volume applications.

      • Chemically resistant materials: Constructed with a polymer cover and base, chemically resistant tubing, and an inert carbon fiber arm for better compatibility with a wide range of sample matrices.

      • Automated rinsing: An integrated flowing rinse station with an on-board peristaltic pump reduces carryover and cross-contamination between samples. An optional dual rinse station is available.

      • Accurate positioning: High-resolution XYZ movement ensures precise and repeatable probe placement. 

Sample types and applications:

• • • • The Shimadzu ICP-MS 2030LF with the Teledyne ASX-280 is suitable for a broad spectrum of liquid sample matrices across several industries. The HFS-5 option is available for samples containing hydrofluoric acid. 

Common sample types include:

• • • • Aqueous solutions: For environmental monitoring, such as drinking water and wastewater analysis.

      • Acid-digested solids: For food and agricultural products, biological samples, and other materials where elements are extracted into a liquid medium.

      • Organic solvents: The system can be configured to introduce organic solvents, with argon and oxygen added to prevent carbon precipitation.

      • Hydrofluoric acid (HF) containing samples: The optional HFS-5 system allows for the direct injection of samples containing HF. 

      • Key applications include:

      • Environmental testing: Monitoring trace and toxic elements in water and soil extracts.

      • Food and agriculture: Analyzing essential and hazardous elements in food products, such as minerals and heavy metals in infant formula.

      • Pharmaceuticals: Measuring elemental impurities to comply with regulations like ICH Q3D and FDA 21 CFR Part 11.

      • Cannabis testing: Analyzing for heavy metals and other trace elements.

      • Materials science: Elemental analysis of extractables from materials like plastics.