Rigaku XtaLAB mini Benchtop Single Crystal X-Ray Diffraction with Cryo-cooling

Rigaku XtaLAB mini Benchtop Single Crystal X-Ray Diffraction with Cryo-cooling (Armstrong Campus) (CCRL14)

Located in room 2018 in the Science Center.

Below the specifications is the calendar to schedule appointments, and below that is the calendar showing all already scheduled reservations:

You must be logged into a @georgiasouthern.edu or Gmail account to reserve instrument time.

The Rigaku XtaLAB mini II, especially when equipped with a cryo-cooling system, is primarily designed for single crystal X-ray diffraction (SC-XRD) of small molecules. The cryo-cooling option allows for the collection of data at low temperatures.

Here's a breakdown of the samples and capabilities:

Sample Types:

Small Molecule Single Crystals: The XtaLAB mini II is specifically designed to work with small molecule single crystals to determine their 3D structures.
Organic Materials: When equipped with a cryo-cooling stage, it can be used to investigate organic materials, particularly at low 2θ angles.

Capabilities:

Single Crystal Structure Determination: It can determine the 3D structures of small molecules to a publication-quality standard.
Benchtop Operation: Its compact size allows it to be placed on a standard lab bench, making it accessible to individual research groups.
Low-Temperature Data Collection: The optional cryo-cooling system (e.g., Oxford Cryostream 800) enables data collection at low temperatures, which can be useful for studying temperature-sensitive materials or improving data quality.
User-Friendly Software: It comes with CrysAlisPro software for data collection and processing, with automated features like crystal screening and structure solution.
Reduced Size, Undiminished Quality: Despite its compact size, the XtaLAB mini II maintains research-grade data quality for accurate structural determination.
"What is this?" Feature: This feature allows for rapid sample identification before committing to a full data collection.

In essence, the XtaLAB mini II with cryo-cooling is a valuable tool for chemists and material scientists who need to determine the structures of their synthesized compounds or investigate the behavior of materials at low temperatures. The optional cryo-cooling system expands its utility for studies involving temperature-dependent phenomena or working with crystals that diffract weakly at room temperature.

User document(s) for Single Crystal XRD Software:

1 - CrysAlis Pro (CAP) Quick User Guide

2 - CrysAlis Pro (CAP) Procedures for creating a crystal movie and absorption correction model.

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