JEOL 300 MHz NMR

Charges: $30/hour, $20/hour off peak,  External users $50/hour - 3 hour cap

(Future charges subject to change)

The JEOL JNM-ECS 300 MHz NMR spectrometer is a versatile instrument primarily used for analytical and research applications. It's suitable for routine analysis and structural determination of a wide range of samples. 

Specifically, it can be used for:

• Liquids/Solution samples: The instrument delivers high-resolution NMR spectra for liquids and solutions.

• Solid samples: The JNM-ECS can also be utilized for solid-state NMR measurements.

• Organic compounds: It's an ideal instrument for structural analysis of organic compounds and is frequently used in organic chemistry.

• Natural products: JEOL NMR spectrometers, including the ECS series, have a long history of use in analyzing natural products.

• Polymers: The JNM-ECS series can be employed for polymer research, and optional accessories like the Pre-Heat ASC30 are available for handling high-temperature polymer samples.

• Biotechnology and Food Analysis: It can analyze bio-solutions, study molecular composition in biotechnology, and identify and quantify contaminants or nutritional components in food samples.

• Pharmaceutical research, Materials science, and Biochemical analysis: These research domains frequently utilize the JNM-ECS spectrometer for molecular structure determination, compound purity assessment, reaction mechanism studies, and advanced structural characterization. 

Capabilities of the JEOL JNM-ECS 300 MHz NMR spectrometer include:

• High-resolution NMR spectra: It features a 300 MHz superconducting magnet and delivers high-resolution NMR spectra for various applications.

• Multi-nuclear observation: The Royal probe (RO5AT/FGSQ) allows for observation of a variety of nuclei. The low-band coil can be tuned to observe nuclei from 31P to 15N, as well as 39K and 109Ag. The high-band coil can be tuned to 1H or 19F.

• 1D and 2D NMR experiments: It's suitable for acquiring both direct and indirect detection 1D and 2D NMR spectra, including experiments like COSY, NOESY, ROESY, HSQC, and HMBC.

• Variable temperature capabilities: It can perform experiments within a variable temperature range of -100°C to +150°C.

• Automation: The JNM-ECS can automatically perform multiple experiments on different samples with features like auto-tuning and auto sample changers.

• Gradient shimming: The Royal probe includes a single Z-axis gradient coil, and gradient shimming can be performed on various nuclei, including 19F and 2H.

• High sensitivity: The JNM-ECS boasts high 1H and 13C sensitivity, enabling rapid analysis.

• Software and networking: It utilizes Delta software for control and processing, and the spectrometer can be networked for remote operation. 

In summary, the JEOL JNM-ECS 300 MHz NMR spectrometer is a powerful and versatile instrument suitable for a wide range of analytical and research applications in various fields, with capabilities for both liquid and solid samples, multi-nuclear observation, 1D and 2D experiments, variable temperature control, automation, and high sensitivity.

User document(s) for NMR Software:

1 - Instrument operating instructions and use of Delta software.

2 - Data processing with Delta software.