Miniaturized Magnetic Stirrer
University of California, San Diego
Sponsored by IKA
Background
IKA is a leading company in the production of laboratory equipment and technology. With headquarters based in Staufen, Germany and branches in four different continents, IKA designs and produces lab equipment ranging from hot plates to shakers to magnetic stirrers. One of IKA's best-selling products is the IKA lab disc, a slim magnetic stirrer that uses magnetic coil technology allowing for the stirring of 50ml+ solutions with minimal space impact.
MAE 156B Spring 2017 Sponsored Project
IKA Lab Disc
http://www.ika.com/owa/ika/catalog.product_detail?iProduct=3907500
Objective
Design and fabricate a magnetic stirrer capable of stirring multiple small vials (0.5-5ml) of solutions with viscosities similar to that of water. The specific requirements are as follows:
Four stirring positions minimum
50mm x 50mm x 5mm maximum size for 4 coil array
300 rpm to 1500 rpm stirring speed
5mm thickness maximum for entire device housing
Further, explore the possibilities for mobile app-control, battery power, inductance charging and modular communication.
Components
Magnetic Plates and Cores
Guide the magnetic field lines
Diagonally adjacent Top Plates behave as opposite poles
Bottom Plate confines magnetic field lines to the top surface
Higher Relative Magnetic Permeability = Stronger Magnetic Field
Table 2. Magnetic permeability and relative cost of materials
1008 Low Carbon Steel
Low Cost
Machined on CNC Lathe
(3.72mmH x 3mmD)
1018 Low Carbon Steel
Low Cost
Cut on Waterjet
The Battery Powered module Coils draw only 400mA to ensure a sustainable battery life.
The Bluetooth Enabled module Coils draw approximately 600mA.
High enough resistance for current draw to ensure sustainable battery life
Low resistance creates strong magnetic field with low voltage
Eliminates the need for a bobbin
Utilizes extra height for more wire turns
In our efforts to reduce the height of our device, our sponsor suggested dissolving the ABS bobbins to further shave off 1mm of height from the coils. We decided to implement this suggestion by gluing the coils in after spooling to allow it to retain its shape and then dissolve the ABS bobbins using Acetone. We successfully tested this method on a single coil and verified that the magnetic wire retains its enamel.
Dissolving ABS Plastic with Acetone
Remaining Coil Sealed with Polyurethane Adhesive
Adafruit Pro Trinket: Microcontroller
Adafruit Powerboost 500: Used to step up 3.7V from battery to 5V used by H-bridge
Adafruit L293D H-Bridge: Allows polarity of coils to be reversed
Adafruit 3.7 V Lithium Ion Polymer Battery: Powers module
Raspberry Pi Zero: Microcontroller with Bluetooth functionality
Adafruit L293D H-Bridge: Allows polarity of coils to be reversed
Casing
Design Requirements:
9 mm thick for Battery Powered module
5 mm thick for Bluetooth Enabled module
Component mounts
Channels for wiring
Ports for power supply
Future designs to be aluminum cut or injection molded
Egonomic design for consumers
CAD of Front, Back & Section Views: Battery Powered Module & Bluetooth Module
Final Design & Performance
Battery Powered Module
Bluetooth Enabled Module
Battery Powered Module
Bluetooth Enabled Module
CAD of Battery Powered Module
Wireless
Fully Battery Powered
6.5-7.5 hours Battery Life
Four Stirring Positions
Variable Speed Control
Inductive Charging
CAD of Bluetooth Enabled Module
Wired
Bluetooth control through mobile phone app
Faster stirring speeds achieved
Four Stirring Positions
Variable Speed Control
Convex bottomed vials decouple at 1000 rpm
Flat bottomed vials decouple at 1500 rpm
Convex bottomed vials decouple at 1500 rpm
Flat bottomed vials decouple at >1500 rpm
Median Decoupling Speed of Stirrer in Varying Configurations
Implementation of custom PCB and microcontroller
Reduce overall size
PCB Printed Coils
Reduce volumetric footprint
Increase portability and ease of transport
Higher magnetic permeability materials for cores and plates
Reduce size of coils needed
Decrease the current draw from the power source
Possibility of a Card-thickness module with a appropriate material (Pure Iron 99.99% Hydrogen annealed)
Double Wrapped Coils
Twice the Magnetic Field and half the resistance
Lower the amount of voltage needed for a higher field
Draft Angles on Housing
To easily separate an injection molded housing
Prototypes
The initial risk reduction verified that we could quickly and inexpensively produce prototype magnetic coils.
Risk Reduction Test Bed
The second prototype successfully implemented stirring of a single vial using four coils.
Circuit Schematic Diagram
The next few prototypes focused on testing the difference between using wires of varying gauge size.
Before implementing the 9-coil array, a 6-coil array with 2 stirring positions was built to quickly find out possible issues with sharing magnetic coils between stirring positions.
The next few prototypes successfully implemented 4 position stirring using a 9-coil array. It was observed that although three vials could be reliably stirred simultaneously, the addition of the fourth vial caused the negihbouring stir bars to decouple from the coils. The system was also highly sensitive to the positioning of the vials.
CAD of proposed Magnetic Plate & Core design
The distance at which the magnetic stir bars interfere was determined to be approximately 25mm apart by physically moving one vial closer to the other on our prototype as it was stirring. Based on this measurement, the coil and bobbin dimensions were redesigned using a CAD template as reference and the coils were packed as close as possible without causing interference.
CAD Schematic of Coils, Vials & Grid Layout
The Pattern of the plates were also experimented with and tested relative to one another.
Star Pattern Upper Plates & Circle Pattern Lower Plate
Rectangluar Pattern Upper Plates
9 Coil ABS Dissolved Bobbin Prototype