In this study, we will present the synthesis process for LiNi0.85Mn0.075Co0.075O2 by co-precipitation method (adopted industrially), which is optimized very carefully with respect to pH, temperature, as well as concentration of the reactants, etc. This material has been engineered to have a better capacity and capacity retention using the optimization of the calcination temperature. This material was further characterized by PXRD (powdered x-ray diffraction), ICP-OES (inductive coupled plasma-optical emission spectrometry), SEM (scanning electron microscopy), and electrochemical performance using galvanostatic charge-discharge cycling technique.