DESCRIPTION: a BRUKER AVANCE IIIHD 600MHz system equipped with a 5mm H/F-TCI CryoProbe and SampleJet sample changer.
The 5mm H/F-TCI CryoProbe with SampleJet can handle 5mm, 3mm and 1.7 tube sizes.
The Bruker 600 runs TopSpin3 and is used for running both small molecules and biomolecules with high sensitivity and the capability for running multiple samples under automated control via IconNMR and a SampleJet sample changer
USER COST: see Documents, Fees, Supplies and Services
SCHEDULE TIME AND RULES: NMR Instrument Schedules and Reservations
NMR SAMPLE PREPARATION GUIDE: see NMR Sample Prep Info for EinsteinNMR
SAMPLEJET GUIDE: see SampleJet Info
IconNMR GUIDE: see IconNMR Info (useful for automated set-up, acquisition and processing of routine experiments)
DOCUMENTS:
Instructions for acquiring 1D 1H and 13C spectra on the Bruker AV600 5mmCryoTCI probe using TopSpin (instructions for set-up and acquisition of experiments manually; for routine experiments, it is recommended to use IconNMR instead)
ACKNOWLEDGEMENT: Please include statement in the acknowledgement section when publishing data collected on the instrument; see following for details: Acknowledgement Info For Publications
NOTICES AND OPERATIONAL NOTES: Bruker 600 Notices and Operational Notes
SENSITIVITY OF 5mmCryoH/F-TCI cryoprobe (Z129649/0016 CP TCI 600S3 H&F-C/N-D-05 Z):
1D 13C for ~5mg sample will take about 10-15 min.
13C_SINO=1406 (3/18/2014; Acceptance Test on ASTM; 129649_0016sna #100)
1H_SINO=6466, 2ppm noise (3/8/2014; Acceptance Test on EB; 129649_0016snh #100)
1H_SINO=1202 (3/17/2014; Acceptance Test on 2mM Sucrose; 129649_0016ws #7)
TEMPERATURE RANGE OF 5mmCryoH/F-TCI cryoprobe: -0 C to 80 C
NOTE: PLEASE CONSULT STAFF IF YOU WISH TO RUN SPECTRA BELOW 10 C or ABOVE 50 C (make sure your solvent FP is below and BP is above the temperature you wish to run at!)