DESCRIPTION: a BRUKER AVANCE IIIHD 300MHz system equipped with a 5mm BBFO probe and SampleCase sample changer.
The 5mm BBFO probe with SampleCase can handle 5mm tubes.
The Bruker 300 runs TopSpin3 and is used for standard 1H/13C on small molecules.
STANDARD COST FOR EINSTEIN USERS: $5/hour
SCHEDULE TIME AND RULES: NMR Instrument Schedules and Reservations
NMR SAMPLE PREPARATION: see NMR Sample Prep Info for EinsteinNMR
SampleCase Sample Changer GUIDE: SampleCase Instructions for EinsteinNMR Users
IconNMR GUIDE: see IconNMR Info (useful for automated set-up, acquisition and processing of routine experiments)
DOCUMENTS:
Instructions for Acquiring Spectra on the Bruker AV300 5mmBBFO probe using TopSpin (instructions for set-up and acquisition of experiments manually; for routine experiments, it is recommended to use IconNMR instead)
SENSITIVITY OF 5mm BBFO probe (Z104275/0281 PA BBO 300S1 BBF-H-D-05 Z) :
1D 13C for ~5mg sample will take >1 hour.
13C_SINO=121 (10/8/2013; Acceptance Test on ASTM; 104275_0281sna)
1H_SINO=187, 2ppm noise (10/8/2013; Acceptance Test on EB; 104275_0281snh)
Users needing 13C, 19F on dilute samples (<5mg) should consider using the 5mmCryoH/F-TCI probe on the Bruker 600 MHz NMR Instrument.
TEMPERATURE RANGE OF 5mm BBFO probe: -150 C to 150 C (applies only with shim system temperature range of 0 C to 80 C)
NOTE: PLEASE CONSULT STAFF IF YOU WISH TO RUN SPECTRA BELOW 10 C or ABOVE 50 C (make sure your solvent FP is below and BP is above the temperature you wish to run at!)
CONFIGURATIONS: Please see staff if you wish to change the probe configuration. The following probes are available for installation:
5mmBBFO
5mmBBI