Upon completion of this experiment, students will:
(CLO) Analyze evidence to decide if generalizations or conclusions based on the obtained data are warranted
(MLO1-1) Utilize algebraic methods, scientific notation, rounding numbers, and significant figure rules in calculations
(MLO1-2)Apply units of mass, temperature, time, length, and derived units, such as volume and density using dimensional analysis to solve problems with single or multiple steps or conversions. Recall the common base SI units of measurement, prefixes, and their associated symbols
(MLO1-3) Evaluate the uncertainty, accuracy, and precision of measurements.
Use best practices to maintain a safe laboratory environment
Interpret a Safety Data Sheet and chemical hazard label.
Recognize common glassware and equipment used to make measurements with proper significant figures and units
Become familiar with the safe operation of a Bunsen burner
Experiment 0 covers best practices, safety protocols and an introduction to laboratory equipment and their proper use.
The assignments that must be completed are the following:
Part I - Safety in the Laboratory.
Watch the Starting with Safety Video
Complete the Laboratory Safety Agreement
Complete the Safety Quiz in Canvas
Part II - Use of Safety Data Sheet Report
Part III - Common Glassware and Laboratory Equipment Quiz in Canvas
Part IV - Use of Tools to make Measurements Report
Part V - The Bunsen Burner report
Each of these assignments count toward the laboratory grade.
Links to the assignments and resources are below.
This is the Google Slides Experiment 0 Presentation
The discussion of this laboratory material is in the complete laboratory assignment above for each of the five parts of the laboratory assignment.
A summary of the procedures and the report sheets that need to be completed are below.
Complete the individual parts of this laboratory using the resources given below and in the laboratory assignment.
Introduction and Discussion:
Safety in the laboratory is a priority that everyone must participate to ensure a fun and fulfilling experience. The chemistry laboratory is inherently filled with possible dangers. Equipment, materials, and chemicals all have possible safety concerns. Every person in the laboratory is responsible for their own safety and for the safety of the group. In this experiment, you will watch a video about safety in the laboratory and then discuss the rules and consequences of not following these rules when situations arise while working in the chemistry laboratory.
Discussion of Safety and Safety Equipment:
Safety in the laboratory can be classified into several categories, personal safety which includes investigation of any chemicals that will be used and the dangers the chemical may possess; personal behavior in the laboratory setting, first aid and response to emergencies.
Good laboratory practices are the industrial standard for maintaining a proper laboratory environment. You should read the Safety rules in Part I of Experiment 0 and Appendix B - Clean Laboratory Practice and then watch the following videos on Safety.
This is the Laboratory Safety Agreement.
Complete this assignment by downloading the Laboratory Safety Agreement initialing each page, signing the agreement and posting the document to the assignment in Canvas.
Watch this Safety video
https://youtu.be/0zHev9iM8kU Although this video is dated, it covers all of the topics that should be understood to work safely in the laboratory. The video was produced by the American Chemical Society.
Proper Dress and PPE (Personal Protective Equipment) / Lab Safety Video
Part 1 - http://youtu.be/GjAD83B4JaY
Safety Equipment / Lab Safety Video
Part 2 - http://youtu.be/IiHEYtnKfF0
Behavior / Lab Safety Video
Part 3 - http://youtu.be/e7VkIuiT1kU
Chemical Hazards / Lab Safety Video
Part 4 - http://youtu.be/8queMM7VVfw
Safe Chemical Handling / Lab Safety Video
Part 5 - http://youtu.be/uiB8qnlZTAM
Other General Hazards / Lab Safety Video
Part 6 - http://youtu.be/q8UiamEWz4Q
Flinn Scientific Safety Review: http://youtu.be/V-fNpaOX0-g
Complete the Experiment 0 Part II Report
Teachers, students, custodians, and other staff may be exposed to hazardous materials at any time. Such exposure can cause or contribute to serious health effects, such as effects on the nervous systems, kidney or lung damage, sterility, cancer, burns, and rashes. In addition, some hazardous materials may pose immediate physical or chemical risks, such as causing a fire or an explosion. There are three major components to understanding the chemical you will use
Labels applied to containers of hazardous materials. The labels alert the user to the dangers of the product and to the essential precautions for its safe use.
Safety Data Sheets (SDS) must be prepared by the product supplier and supplied to the user. These sheets provide detailed information about product composition, reactivity, health effects, protective equipment and procedures, and emergency procedures.
Education and Training related to hazards and associated safe work procedures is mandatory for those either working with or working in the proximity of the controlled product.
Watch the video above called Chemical Hazards (4) . The video talks about the SDS and labeling used for chemicals in the lab.
Perform a search for the SDS of the compound assigned and complete the Use of Safety Data Sheets.
Resources for SDS:
An easy way to search for a Safety Data Sheet is to simply google it. by typing in "SDS name of compound". Look for an SDS that is published by a manufacturer or company and contains a company logo.
A search engine by Ward Scientific: https://wardsci.com/cms/how_to_read_and_use_SDS
The American Chemical Society on What is a Safety Data Sheet? https://www.acs.org/content/acs/en/chemical-safety/basics/safety-data-sheets.html
Complete the Use of Safety Data Sheet and Labeling Report
Glassware and equipment is essential to the successful completion of the laboratory assignments. Part II of this lab focuses on the types of glassware or equipment used in the lab. In the laboratory, we use tools, glassware and equipment regularly. The student should be familiar with all the equipment and how to use it properly.
There are five basic types of measurement we will perform in the lab.
mass
volume
length
temperature
time
The equipment and glassware we will use in the lab to make these measurements is described in the laboratory assignment. There are many assessments and resources online to help you identify the glassware and equipment we will be using in the laboratory,
This is a link to help you study for the glassware and equipment quiz in Canvas. http://www.sciencegeek.net/Chemistry/taters/labequipment.htm (This is NOT the quiz or assessment you must complete for this assignment.)
Basic Chemistry Lab Equipment: https://youtu.be/_A3JxpMU63s
Complete the Experiment 0 Part IV Report
In this part of the experiment, we will use various tools in the laboratory to collect data and analyze the values.
Measurement in the laboratory is how we collect data. The tools we use have defined precision based upon the scale represented on the tool. To be able to read the tool with the proper precision, the student must understand the scale. Unit also provide information about the measurement, no number should be represented without a description or a unit.
When a tool is used the ability to make the measurement is dependent upon the markings, gradation or scale used on the tool. Precision of the measurement is indicated by the number of values or decimal places represented by the scale of the tool.
This is the experiment 0 part IV report and procedure. The directions for completing this assignment are at the end of this document
This is my explanation of scales and gradations for this experiment
What are scales or gradations and How to Read Scales
The importance of reporting a measurement properly
Using a single object, weigh the object on 4 different balances, Determine the average and average deviation of the four masses. Consider: Are all the masses the same? Why are there differences? A balance has precision based upon the number of decimal places it displays for the mass, but the precision of the mass is determined by the average deviation which shows how close each mass is to the average value or to each other.
The proper use of the analytical balance will be described by your instructor. Every balance should always be left clean, any materials spilled wiped up. The doors on an analytical balance should be closed during and after your measurement. Obtain an object and measure the mass on each of the analytical or pan balances provided. Report the mass to the proper significant figures. Compare the mass taken on each balance; calculate a mean or average mass and the average deviation. Report the answer to the proper significant figures.
This is an explanation of mass for this experiment.
We use balances to determine the mass. The following videos show the proper use of an Analytical Balance:
We use balances to determine the mass. The following videos show the proper use of an Analytical Balance:
Calculate the average and average deviation of your four masses.
Find the mean or average of a group of numbers
Calculating the mean average deviation
Accuracy and Precision (Part 2)
Add water to a graduated cylinder and study the features of the water’s surface. State a hypothesis for the reason the meniscus forms. Remember a hypothesis is a supposition or proposed explanation made on the basis of limited evidence as a starting point for further investigation.
We will determine the volume of liquid in several different glassware items. Record each volume measurement with the correct number of significant figures and units. Remember to observe the water level at eye level
Volume measurements use various tools, but to make precise measurements we use the following tools.
Using a Buret or a pipet: https://youtu.be/Asg55fFt4zk
how to read a graduated cylinder: https://youtu.be/7ewRaV5baik
Buret Tutorial: https://drive.google.com/open?id=1RgFQPJyeiAMbCiXRn21_U2X2XpeKyyqWDHVzVts2As
In this simulation (https://teachchemistry.org/classroom-resources/measuring-volume-simulation), students will participate in a 10 question quiz. The quiz questions are each made of two parts, with the first part requiring the student to analyze an image of a graduated cylinder in order to report an accurate measurement. Students must use the correct number of significant digits based on the markings presented on the cylinder when reporting the measurement. In the second portion of the question the students will determine the uncertainty value of the graduated cylinder, again by analyzing its markings. The simulation is made up of several different sizes of graduated cylinders, each containing unique markings, so students will be challenged to analyze each individually.
Measuring Volume simulation: https://www.explorelearning.com/index.cfm?method=cResource.dspDetail&ResourceID=1048
This video shows how to read a graduated cylinder of various sizes and different scales.
Watch this video to see how a buret measures liquids.
Buret Tutorial: https://drive.google.com/open?id=1RgFQPJyeiAMbCiXRn21_U2X2XpeKyyqWDHVzVts2As
Measurement of length can be accomplished using several tools.
How to read a standard ruler (in inches): https://youtu.be/H70smlwaKrE
How to read a metric ruler: https://youtu.be/GbOu0d18mSg
How to read a micrometer: https://youtu.be/O8vMFFYNIfo
How to read a caliper: https://youtu.be/MHu_BaYoKfM
This is an explanation of how to use the tools and make the measurements of length for this experiment.
A standard ruler in inches to the left on the ruler and a metric ruler in centimeters to the right above.
The video shows how to read a caliper with a venier scale to the proper significant figures.
This video shows how to use and read a metric micrometer with the proper significant figures.
We can use several types of thermometers, digital, mercury or alcohol thermometers.
Most thermometers that we have in the lab can often read temperature in both the Celsius or the Fahrenheit scales but generally, we always use the Celsius scale in science.
Measure the temperature of water in a beaker using a thermometer.
If you read the Fahrenheit scale, we would need to convert that temperature into Celsius.
The third temperature scale we use in science is Kelvin. The Kelvin scale or Absolute temperature measures the energy of the particles and becomes extremely important when we are looking at the atomic scale of matter. I want you to convert this temperature into Kelvin.
The Bunsen burner was named after the inventor Robert Bunsen. The Bunsen burner is one of the common laboratory equipment that is used to heat or sterilize with a natural gas combustion. How to Use a Bunsen Burner:
The image :http://i235.photobucket.com/albums/ee5/Angelish98/bunsenburnerdiagram.jpg