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Powder X-ray Diffraction. PXRD spectra were collected on a Rigaku Miniflex 600 spectrometer using an copper anode X-ray source. Diffractograms were collected with a 2 theta range of 3 to 90 at a speed of 15 degrees/min and step size of 1.
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This work was performed in part at the Surface Analysis Laboratory in the Department of Chemistry at Virginia Tech.