Niespolo Micro-Analytical Geochronology (NiMAGe) Lab

The NiMAGe Lab hosts three spaces: 

The Chemistry Lab: An ISO Class 6 / FS209E Class 1000 chemistry lab with three ISO Class 4 / FS209E Class 10 vertical laminar flow hoods, weighing station, and related equipment to conduct cation exchange column chromatography for U-Th geochronology


The Mass Spectrometer Lab is an ISO Class 7 / FS209E Class 10,000 clean room and hosts three instruments:

A Thermo Neoma multi-collector inductively coupled plasma mass spectrometer (ICP-MS)

An Agilent 8900 QQQ ICP-MS

An ESI Lasers NWR 193 ImageGEO Laser Ablation system


The Preparation Lab: A space to cut, drill, dremel, sonicate, separate, and epoxy-mount samples. 

Applications

Using the QQQ ICP-MS (and researchers leading this work):

In situ trace element concentration profiling of volcanic glass, carbonate biominerals (eggshells, teeth, corals) (Niespolo, Akhtar)

In situ U-Pb dating of accessory minerals (Apen)

Solution-based geochemical assay of water (Niespolo)

Solution-based measurements of lithium isotopes using cold plasma mode (Weldeghebriel)

Using the Neoma (in progress; and researchers leading this work):

Uranium-series (U-Th) geochronology of carbonates (Niespolo, Salas-Saavedra)

Strontium isotopes by Laser Ablation (LA) ICP-MS (Niespolo)

Split-Stream laser ablation dual ICP-MS to simultaneously measure major and trace elements on the QQQ and a selected isotope system on the Neoma (Niespolo)

Research Themes

I am interested in anchoring paleoclimate and fossil records to absolute timescales to assess correlations of local and global environmental changes to evolution and adaptation.

A Core Research Theme addresses outstanding questions on the timing and tempo of human evolution, the development of modern human behaviors, and the timing of global-scale human colonization. How these are recorded,  what local environments were like during these significant leaps in biological and cultural evolution, and human-environment interactions, drive my research.

In the field, I include landscape survey, sediment and tephra stratigraphy, drill cores, and archaeological excavation to constrain the ages and paleoenvironments of deposits critical to understanding the core research themes.

In the lab, I use a combination of micro-analytical approaches (laser ablation, petrography, electron microscopy, x-ray techniques) and high-precision mass spectrometry for isotope measurements to utilize the optimal sample to answer the geological/chronological question of interest.


I am also interested in understanding crustal processes using petrology and isotope geochemistry, a focus of my M.S. research (see "recent projects" in the Research drop-down menu).