Microscale Laboratory Primer (MLP)
MLP Graphics
Laboratory Grading Rubric + Guidelines
Sample Laboratory Record
Safety, Equipment, Technique, Notebook
Make-Up Videos
Pre-Lab Video
Pre-Lab Slides
Lab #1 - Recrystallization and Melting Point Analysis of Phthalic Acid
Melting Point Analysis Protocol
Distillation Pre-Lab Video
Distillation Pre-Lab Slides
Lab #2 - Simple Distillation of Listerine Mouthwash and Analysis via Gas Chromatography
Gas Chromatography Pre-Lab Video
Gas Chromatography Pre-Lab Slides
Gas Chromatography Protocol
Lab #3 - Extraction, Isolation, and Purification of Caffeine from Tea Leaves
Lab #4 - Thin-Layer Chromatography of Analgesics
Thin-Layer Chromatography Protocol
Lab #5 - Chromatographic and Spectrophotometric Analysis of Plant Pigments
Column Chromatography Protocol
TLC and Spectrophotometry Reference Data
Trans-Fatty Acids + Margarine Reading
Lab #6 - Preparation of Shortening from Olive Oil via Catalytic Transfer Hydrogenation
Post-Lab Discussion
Tips for Yield Analysis
Lab #7 - Diels-Alder Synthesis of a Bridged Bicyclic Ring
Lab #8 - Chiral Resolution of Racemic Phenylsuccinic Acid
Laurent Half-Shade Polarimeter Operating Instructions
Lab #9 - IR and 1H NMR Analysis of a Complex Unknown
Make-Up Data