This course is introduced to give you a reasonable understanding in the major techniques of electroanalytical methods, thermal methods and radioanalytical methods. In this course we will cover the basic theory, the practical aspects and scope of all individual techniques of these three categories. In electroanalytical techniques we use one or more electrical properties under controlled condition to obtain qualitative and quantitative information of a sample. These techniques can be divided into several classes depending on which aspects of the electrochemical cell are controlled and which are measured. You may be familiar with some of the electroanalytical techniques like potentiometry. In this course along with these techniques we will also introduce few new electroanalytical techniques like coulometry and voltametry. All these electroanalytical techniques will be discussed in Blocks 1, 2 and 3. Similar to electrical properties, in thermal methods we study changes in the physical and chemical properties of a sample while it is undergoing heating process. We are also focusing on three important thermal techniques, that is, thermo gravimetric analysis (TGA), differential thermal analysis (DTA) and differential scanning calorimetry (DSC). There techniques are discussed in Block 4. In last block of this course, i.e. Block 5, you will study radioanalytical methods which are unique with regard to theoretical principles involved, handling of radioisotopes, and instrumentation.
Block 1 : Electroanalytical Methods-I
This block starts with introduction to electroanalytical methods and discusses the methods under potentiometry-I and potentiometry-II (pH metry)
Block 2 : Electroanalytical Methods-II
The electroanalytical techniques covered in this block include Conductometry, Electrogravimetry and Coulometry and their applications.
Block 3 : Electroanalytical Methods-III
In this block voltammetry, polarography and amperometric titrations are covered. These instrumental methods of analysis, their methods of operation and their applications are discussed.
Block 4 : Thermal Methods
This block covers analytical methods which are based on the determination of changes in chemical or physical properties of material on heating. These analytical methods are known as thermal methods viz., thermogravimetric analysis, differential thermal analysis, scanning calorimetry and thermal titration.
Block 5 : Radioanalytical Methods
In this block, radio analytical methods are discussed which are unique with regard to theoretical principles involved, handling of radioisotopes, and instrumentation. These methods are based on nuclear properties rather than chemical properties in all other analytical methods described in the previous 4 blocks.