Project Title: Development of scanning Hall probe microscopy for the quantitative study of the stray magnetic fields produced by high performance micro-magnets
Supervisors: Dr. Klaus Hasselbach (MCBT), Dr. Nora Dempsey (QUEST), Institut Néel.
Micro-magnetic devices are developed for application in bio & automobile sensors, etc. The materials in these sensors must be characterized after integration in the device. Scanning Hall probe microscopy (SHPM) is a tool of choice for detecting the stray-field of the packaged devices. In this project, I have developed a SHPM setup at Institut Néel with Dr. Klaus Hasselbach [1]. The setup is being currently utilized for the study of micro-magnet arrays being developed for applications in micro-systems [2-4].
I have also been involved in the micro-magnetic imprinting (µMI) process [2] of fabrication of hard magnetic powder based micro-flux sources (at Institut Néel with Dr. Nora Dempsey). Micro-patterned hard magnetic films serve as templates or master structures in this fabrication process.
I also undertook some modelling of micro-magnetic structures.
In SHPM the Hall sensor measures the z-component of the stray magnetic field emanating from the sample. I have built and used a microscope (development and installation of digital regulation for the microscope and programming user-friendly and reliable LabVIEW software).
Some of the salient features of the SHPM setup are:
The probe is mounted on a quartz tuning fork allowing topographic feedback and constant probe - sample separation. (Scanning at a fixed height without such feedback (flyover mode) is also possible).
Hall crosses of sizes varying between 1-5 µm have been used (Hall probes developed by Prof. Roman Kramer at Institut Néel).
Minimum possible scan resolution given by the stepper motor driven linear stages is 0.1 µm.
Ability to perform scans at various heights from the plane of the sample, from 1 µm up to 35 mm.
Detection of large fields ~ 1 T, such as from strong permanent magnets.
Magnetic field sensitivity ~ 0.1 mT (taking into account the system noise during scanning, but primarily limited by Johnson noise).
Using this microscope, we have studied thin film samples with micro-magnet arrays. The images below show the z-component of the stray field pattern (B) produced at heights of (a) 5 μm, (b) 20 μm, and (c) 50 μm above μMI structures made with crushed melt spun ribbon (average particle size = 5 μm). For each image, scan resolution = 2.5 μm and scan area = 160 × 400 pixels = 400 μm × 1000 μm. The adjoining graph shows B(x) profiles across the dashed lines shown on each image (cf. Ref. [1] for further details).
References:
[[1]] Gorky Shaw et al, Rev. Sci. Instrum. 87, 113702 (2016).
[2] N. M. Dempsey et al, Appl. Phys. Lett. 104, 262401 (2014).
[3] D. Le Roy et al, Mater. Today Commun. 6, 50 (2016).
[4] D. Mitrossilis et al, Nature Communications 8, 13883 (2017).