The Powder X-ray Diffraction Laboratory consists of three instruments:
Equipped with a sealed-tube copper X-ray source and 0D/1D SSD160-2 detector. The instrument can be optionally configured for variable temperature studies, from room temperature to 1,100 °C. System was purchased by Prof. Arthur Mar (CHEM) through an NSERC grant and installed in June 2020.
Equipped with an air-cooled copper X-ray microsource and 0D/1D/2D Eiger 2R-500K detector. The instrument can be optionally configured for (1) variable-temperature studies, from about -180 to 400 °C and (2) structural and other studies on thin films, such as X-ray reflectivity, high-resolution XRD, and grazing incidence XRD. System was purchased by a collective of 9 professors (from CHEM, CME, and EAS departments) through a CFI grant and installed in December 2023.
Equipped with a sealed-tube molybdenum X-ray source and 0D/1D LYNXEYE XE-T detector. The instrument operates in the capillary geometry. System was purchased by a collective of 9 professors (from CHEM, CME, and EAS departments) through a CFI grant and installed in December 2024.
The XRD Lab is located in room E4-10 of the Gunning/Lemieux Chemistry Centre. To arrange access and training, please follow these instructions. If you run into difficulties, please contact Dr. Michael Ferguson (director of the facility) or Dr. Dmitry Vrublevskiy (technician). For researchers external to the Department of Chemistry, please contact Dmitry to discuss arrangements for data collection and/or analysis.
Please note that only authorized users are able to book time on the diffractometer. To reserve an instrument, log in to your Apps@UAlberta account and add a new event in the chemxrd@ualberta.ca (Advance) or chemxrd2@ualberta.ca (Discover) calendar.
Apart from powder X-ray diffraction data acquisition, the facility offers phase identification, peak fitting, structure solution, and structure refinement services.