The principles and applications of mass spectroscopy (excluding features of instrumentation and operation) and interpretation of qualitative and quantitative data, including identification of molecular ion peak, determination of molecular mass and identification of simple fragments
The principles and applications of infrared spectroscopy (IR) (excluding features of instrumentation and operation) and interpretation of qualitative and quantitative data including use of characteristic absorption bands to identify bonds
The principles (including spin energy levels) and applications of proton and carbon-13 nuclear magnetic resonance spectroscopy (NMR) (excluding features of instrumentation and operation); analysis of carbon-13 NMR spectra and use of chemical shifts to determine number and nature of different carbon environments in a simple organic compound; and analysis of high resolution proton NMR spectra to determine the structure of a simple organic compound using chemical shifts, areas under peak and peak splitting patterns (excluding coupling constants) and application of the n+1 rule
Determination of the structures of simple organic compounds using a combination of mass spectrometry (MS), infrared spectroscopy (IR) and proton and carbon-13 nuclear magnetic resonance spectroscopy (NMR) (limited to data analysis)
The principles of chromatography including use of high performance liquid chromatography (HPLC) and construction and use of a calibration curve to determine the concentration of an organic compound in a solution
Determination of the concentration of an organic compound by volumetric analysis, including the principles of direct acid-base and redox titrations (excluding back titrations).
Chapter 10. Analysis of organic compounds, p331-378
Problem solving exercises
Exercise 10.2 Mass spectrometry, page 336-338, problems 1-10
Exercise 10.3 Infrared spectroscopy, page 342-344, problems 1-6
Exercise 10.4 NMR spectroscopy, page 353, problems 1-10
Exercise 10.5 Combining spectroscopic techniques, page 356-358, problems 1-5
Exercise 10.6 Chromatography, 364-365, problems 1-8
Exercise 10.8 Review, page375-385
Volumetric analysis
Mass spectrometry: Bozeman Science
Mass spectrometry: Professor Dave Explains
IR Spectroscopy: Professor Dave Explains
IR Spectroscopy and mass spectrometry - Crash Course Organic Chemistry
How to identify molecules: Proton NMR - Crash Course Organic Chemistry
NMR Spectroscopy: Professor Dave Explains
NMR Practice Problem: Professor Dave Explains
NOTE: at 6:12 he says and writes "upfield", but meant "downfield".
More Practice with H-NMR Spectra: Professor Dave Explains
HPLC: Royal Society of Chemistry
Chemical Detectives app
A great app for practising solving organic structures using mass spec, IR spectroscopy and NMR. The iPhone version of the app does not work with the latest iOS. It is available on the Google Play Store. I assume it works on an Android phone. I can get it to work on a PC using an Android emulator.
Organic structure databases
Doc Brown's Spectra Database - a particularly good site for easy access to structural data for organic compounds. It is organised by analytical technique and by homologous series, and has been developed for high school level chemistry.
NIST Chemistry WebBook - IR and Mass spectra data
Spectral Database - NMR, IR and Mass spectra data