Research and write up a method to test and identify the functional groups in three unknown organic compounds. You will need to bring your practical method to your Core Practical 15 Laboratory session so that you can follow it.
1. Carry out research to develop methods.
2. Perform a risk assessment using up-to-date information before this practical is carried out.
Research and write up a method to test and identify three unknown inorganic compounds. You will need to bring your practical method to your Core Practical 15 Laboratory session so that you can follow it.
1. Carry out research to develop methods.
2. Perform a risk assessment using up-to-date information before this practical is carried out.
Look over previous practicals for methods
Look at Lab 15 for test videos that may help
Look at Core Practical 7 sheet
Include volumes of chemicals and test samples
Include concentrations of chemicals
Include positive test outcomes
● concentrated hydrochloric acid ● 1 mol dm−3 sodium hydroxide ● 1 mol dm−3 nitric acid ● 0.1 mol dm−3 silver nitrate solution ● 1 mol dm−3 ammonia solution ● 1 mol dm−3 dilute hydrochloric acid ● barium chloride solution ● limewater ● bromine water ● sodium carbonate solution ● ethanol ● concentrated sulfuric acid ● four tubs labelled A, B, C and D ● three bottles labelled X, Y and Z ● nichrome wire ● delivery tube ● Bunsen burner and safety mat ● test tubes and bungs ● distilled water ● dropping pipette ● spatula ● boiling tube ● 250 cm3 beaker ● 100 cm3 beaker ● access to a kettle
CPAC 2c- Identifies and controls significant quantitative variables where applicable, and plans approaches to take account of variables that cannot readily be controlled.
· Choose appropriate equipment for measuring solutions
· Choose appropriate equipment for maintaining temperatures
· Hold test tubes in rack
· Check temperatures with thermometer
· Use blue Bunsen flame during flame tests
· Clean wire rod between flame tests
· Use clean test tubes and pipettes for each test
· Keep lab bench tidy and organised
· Work methodically
· Label test tubes
CPAC 2d - Selects appropriate equipment and measurement strategies in order to ensure suitably accurate results.
· Carry out extensive research to plan a practical with a series of tests to identify organic unknowns
· Carry out extensive research to plan a practical with a series of tests to identify inorganic unknowns
· Plan accounts for volumes required
· Plan accounts for appropriate equipment to measure volumes required
· Plan accounts for concentrations required
· Plan accounts for chemicals required
· Plan accounts for appropriate equipment to measure chemicals required
· Plan accounts for conditions required such as exact temperatures
· Plan accounts for equipment needed to provide conditions required such as exact temperatures
· Plan describes how dependent variables will be measured accurately
· Plan is carried out as described
CPAC 5a - Uses appropriate software and/or tools to process data, carry out research and report findings.
· Carry out suitable research online and from written sources about chemical tests and writes up suitable methods, expected outcomes positive and negative, and safety information in own words citing relevant information, facts and figures within the text as necessary.
CPAC 5b – Sources of information are cited demonstrating that research has taken place, supporting planning and conclusions
· Clearly identifies any material that is a direct quote as such.
· Citation within text as necessary
· Use research to support their identification of organic and inorganic unknowns
· Compile a bibliography of texts from which material has been sourced in such a way that the reader may retrieve the information easily.
· Carry out research to support planning by writing a risk assessment to prepare for safety before practical
· Reference Hazcards in a bibliography in such a way that the reader may retrieve the information easily.
Wear goggles.
Concentrated hydrochloric acid, sodium hydroxide and concentrated sulfuric acid are corrosive.
Nitric acid, hydrochloric acid and limewater are irritants.
Barium chloride and bromine water are toxic and irritants.
Ethanol is flammable – do not use it near a lit Bunsen burner.
Pay attention to the hazard warnings on the tubs and bottles of unknown substances. In particular, if anything is marked flammable, do not use anywhere near a lit Bunsen burner. If heating a flammable substance is required then it must be heated by standing it in a beaker of hot water.
Perform a risk assessment using up-to-date information before this practical is carried out.
Disposal: All the ammoniacal silver nitrate solution should be washed down the foulwater drain with plenty of water. It must not be stored – silver filaments form, which have been known to explode.
CPAC 3a - Identifies hazards and assesses risks associated with these hazards, making safety adjustments as necessary, when carrying out experimental techniques and procedures in the lab or field.
· Complete a sufficient risk assessment prior to task
1. Include chemical hazards reactants & products plus physical hazards
2. Take account of volumes used to ensure risk assessment is appropriate
3. Take account of concentrations used to ensure risk assessment is appropriate
4. Make appropriate assessment made of hazards and risks to do with the practical procedure itself
5. Reference hazcards used to plan for safety (CPAC 5b may be awarded if referenced
Consult CLEAPSS Hazcards® Consult CLEAPSS Hazcards® 6,10A,15B,40A,47A,67,87,91A, 95A,98A,98B,26,19A, 55B, 45C, 83, 38A. Perform a risk assessment using up-to-date information before this practical is carried out