Equipment
boiling tube ● stand and clamp ● bung fitted with delivery tube to fit boiling tube ● water bath for gas collection ● 100 cm3 measuring cylinder ● 50 cm3 measuring cylinder ● test tube ● mass balance (2 d.p.) ● 1 mol dm−3 ethanoic acid ● Powdered calcium carbonate
1. Place 30 cm3 of 1 mol dm−3 ethanoic acid in the boiling tube.
2. Set the apparatus up as shown in the diagram.
3. Place approximately 0.05 g of calcium carbonate in a test tube.
4. Weigh the test tube and its contents accurately.
5. Remove the bung from the boiling tube and tip the calcium carbonate into the boiling tube. Quickly replace the bung in the boiling tube.
6. Once the reaction is over, measure the volume of gas collected in the measuring cylinder.
7. Reweigh the test tube that had contained the calcium carbonate.
8. Repeat the experiment six more times, increasing the mass of calcium carbonate by about 0.05 g each time. Do not exceed 0.40 g of calcium carbonate.
CPAC 2c - Identifies and controls significant quantitative variables where applicable, and plans approaches to take account of variables that cannot readily be controlled.
· Select the correct size cylinder and equipment as in diagram OR chooses to set up a gas syringe
· Correctly weigh test tube before and after addition of calcium carbonate
· Record weigh of calcium carbonate weighed out
· Record weight of calcium carbonate added
· Measure the volume of gas produced to 0.5 cm3
· Carry out 6 repeats with increasing mass of appropriate values
Plan is carried out as described
During this practical activity you must:
Wear eye protection.
Ensure the delivery tube does not become blocked.
Ethanoic acid will sting if it gets into cuts in the skin.
CPAC 3b - Uses appropriate safety equipment and approaches to minimise risks with minimal prompting.
· Collect all eqpt at start to minimise walking around the lab once practical work
· Set up work space in an organised fashion
· Wear safety goggles & lab coats throughout
· No spillages/deals with spillages appropriately with minimal fuss
· Keep stoppers on bottles when not in use
· Hold boiling tubes in racks or clamp (to prevent rolling off the table & smashing)
· Measure out powders next to balance to prevent walking around lab with bottles/open containers of powders
· Correct disposal of reaction mixture (reagents & products) at end of practical
· Area cleared away properly & cleaned down (if needed) for following students without prompting
Consult CLEAPSS Hazcards® 38A &19B . Perform a risk assessment using up-to-date information before this practical is carried out