Embedded Files
For instructor access only: Google Doc for editing the above table available here
Useful Lab Links
Useful Lab Links
Data Table Information
Prelab Data Table template
PDF (for filling in by hand)
Microsoft Word (for filling in electronically)
Useful reference sites for preparing your data table
Useful reference sites for preparing your data table
Use Marvin Sketch software to predict molar mass, etc.
Safety equipment to be purchased
Safety equipment to be purchased
Additional Links
Additional Links
Help with uploading lab reports to Canvas/TurnItIn can be found here
Lab Video (the videos below were prepared by Prof. Jane Wissinger at the University of Minnesota)
Miscellaneous Videos
Miscellaneous Videos
Distillation
Simple Distillation Pt1 - Building the Apparatus https://www.youtube.com/watch?v=n1pnvWgO34A&feature=youtu.be
Simple Distillation Pt2 - Preparing for the Distillation https://www.youtube.com/watch?v=Hhlem2N43S0&feature=youtu.be
Simple Distillation Pt3 - Performing the Distillation https://www.youtube.com/watch?v=QA7nA09lVOw
Tip (use a variac!) https://www.youtube.com/watch?v=_X8LtZ2GgrI
Fractional Distillation https://www.youtube.com/watch?v=ceaOFiB1DMI
Steam Distillation https://www.youtube.com/watch?v=mYC52AR6Iv8
Filtration
Gravity Filtration https://www.youtube.com/watch?v=SxmmxXTTnWA
Vacuum Filtration https://www.youtube.com/watch?v=fz8KJrZT6uc
Extraction
Liquid-Liquid Extraction https://www.youtube.com/watch?v=8bZl7mcG0Ew
Acid-Base Extraction Technique https://www.youtube.com/watch?v=2GuDxHAAuaw
Tips for Neutralizing Extraction Phases https://www.youtube.com/watch?v=Uy0mZ1jrRbQ&feature=youtu.be
Tips for Separatory Funnel Handling https://www.youtube.com/watch?v=Odc1IqiX62k&feature=youtu.be
Chromatography
Thin Layer Chromatography https://www.youtube.com/watch?v=bO05W_Io34Y
How to slurry pack a column https://www.youtube.com/watch?v=IXn0Mfp_gII
Loading a sample onto column https://www.youtube.com/watch?v=LVOkvLPp1gA
Pulling Capillary Tubes https://www.youtube.com/watch?v=Osp8DpPp3is
Introduction to Gas Chromatography (GC) https://www.youtube.com/watch?v=ZpPzImDSfqc
Spectroscopy/Characterization
Packing a melting point tube https://www.youtube.com/watch?v=zzsQkVYRq_g&feature=youtu.be
Preparing an IR sample https://www.youtube.com/watch?v=UqrF5Yu2Xko
Preparing an NMR sample http://youtu.be/khylGw5yPx8
Cleaning up / Waste
Washing glassware https://www.youtube.com/watch?v=gwkyfiPQShw
Handling Lab Waste https://www.youtube.com/watch?v=_-UXFY5iNME
Other techniques
Recrystallization https://www.youtube.com/watch?v=0CoDEBTcXbk
Greasing around glass joints https://www.youtube.com/watch?v=Eau5LvPwJSY
Flame Drying the Grignard Apparatus https://www.youtube.com/watch?v=9G7-Rc4lBcs
Refluxing the Reaction https://www.youtube.com/watch?v=YWISe-8T2BI
Drying of Organic Liquids https://www.youtube.com/watch?v=66QmPP0vluk
(older version: https://docs.google.com/document/d/1cSHFMiX9HKUn4xfuLF3RWNfQYiJS9V4o0kM24NJ6LwQ/edit?usp=sharing)
Lab Video (the videos below were prepared by Prof. Jane Wissinger at the University of Minnesota)
Distillation
Simple Distillation Pt1 - Building the Apparatus https://www.youtube.com/watch?v=n1pnvWgO34A&feature=youtu.be
Simple Distillation Pt2 - Preparing for the Distillation https://www.youtube.com/watch?v=Hhlem2N43S0&feature=youtu.be
Simple Distillation Pt3 - Performing the Distillation https://www.youtube.com/watch?v=QA7nA09lVOw
Tip (use a variac!) https://www.youtube.com/watch?v=_X8LtZ2GgrI
Fractional Distillation https://www.youtube.com/watch?v=ceaOFiB1DMI
Steam Distillation https://www.youtube.com/watch?v=mYC52AR6Iv8
Filtration
Gravity Filtration https://www.youtube.com/watch?v=SxmmxXTTnWA
Vacuum Filtration https://www.youtube.com/watch?v=fz8KJrZT6uc
Extraction
Liquid-Liquid Extraction https://www.youtube.com/watch?v=8bZl7mcG0Ew
Acid-Base Extraction Technique https://www.youtube.com/watch?v=2GuDxHAAuaw
Tips for Neutralizing Extraction Phases https://www.youtube.com/watch?v=Uy0mZ1jrRbQ&feature=youtu.be
Tips for Separatory Funnel Handling https://www.youtube.com/watch?v=Odc1IqiX62k&feature=youtu.be
Chromatography
Thin Layer Chromatography https://www.youtube.com/watch?v=bO05W_Io34Y
How to slurry pack a column https://www.youtube.com/watch?v=IXn0Mfp_gII
Loading a sample onto column https://www.youtube.com/watch?v=LVOkvLPp1gA
Pulling Capillary Tubes https://www.youtube.com/watch?v=Osp8DpPp3is
Introduction to Gas Chromatography (GC) https://www.youtube.com/watch?v=ZpPzImDSfqc
Spectroscopy/Characterization
Packing a melting point tube https://www.youtube.com/watch?v=zzsQkVYRq_g&feature=youtu.be
Preparing an IR sample https://www.youtube.com/watch?v=UqrF5Yu2Xko
Preparing an NMR sample http://youtu.be/khylGw5yPx8
Cleaning up / Waste
Washing glassware https://www.youtube.com/watch?v=gwkyfiPQShw
Handling Lab Waste https://www.youtube.com/watch?v=_-UXFY5iNME
Miscellaneous
Recrystallization https://www.youtube.com/watch?v=0CoDEBTcXbk
Greasing around glass joints https://www.youtube.com/watch?v=Eau5LvPwJSY
Flame Drying the Grignard Apparatus https://www.youtube.com/watch?v=9G7-Rc4lBcs
Refluxing the Reaction https://www.youtube.com/watch?v=YWISe-8T2BI
Drying of Organic Liquids https://www.youtube.com/watch?v=66QmPP0vluk
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