Portland cement, the most important constituent of traditional concrete is responsible for roughly 8% of global anthropogenic CO2 emissions. To curb climate change, the construction industry must transition to low-carbon alternatives, such as replacing traditional clinker with, for instance, abundant clay and limestone.
However, these low CO2 cements suffer from a major drawback: they harden too slowly in the first three days, making them difficult to use on fast-moving building sites.
To solve this, we cannot just look at cement after it has hardened; we need to watch it change live. Standard laboratory microscopes cannot see through dense cement pastes, nor do they have the resolution to see features smaller than a micrometer.
A synchrotron acts as an incredibly powerful microscope. By accelerating electrons close to the speed of light, it generates X-rays that are billions of times brighter than those used in hospitals.
Unparalleled Spatial Resolution (<100 nm): Allows us to see sub-micron structures like C-S-H gel needles and the tiny "etch-pits" forming as cement dissolves.
Rapid Temporal Resolution (<100 minutes): Allows us to take rapid 3D scans over time, creating a 4D movie of a single cement grain as it reacts with water.
By analysing these 4D movies, syn4cem is designing chemical accelerators that will make sustainable concrete harden just as fast as traditional concrete—removing the final barrier to its global adoption.
Syn4cem members at ESRF (from left clockwise) postdoc Shiva, ERC-Adv. Grant awardee M.A Garcia Aranda, ESRF postdoc Victor Okumko , and ReMade@ARI junior scientist Zhenggang Zhang and Ning LiÂ
Ning Li was also with the syn4cem team taking full advantage of ReMade@ARI for his MSCA project Syn4WCO2-CemÂ
ESRF - May 2026
07/05 to 11/05 2026Â
XA-32 "Carbonated Recycled Concrete Fines as Supplemantary Cementitious Materials"Â
beamline: ID19
The ReMade@ARI project is providing for scientists exploring the properties and structures of recyclable materials with a wide range of tailored services at ESRF
Ning Li (left) also joined the team for his own experiments on his MSCA- beneficiary project Syn4WCO2-CemÂ
Over the next two years under the supervision of Prof. M. A. Aranda Ning will be working at the UMA on his project which aligns closely with the European Green Deal, aiming to advance a circular economy within the construction sector.
Â
22/09/25 - 27/09/25Â
proposal ID: 20250412Â
beamline: ANATOMIX
Bridging the gap between micro- and nano-imaging: 4D tomography of cement hydration with the highest possible spatial resolution
08/07/2025Â - 11/07/2025
proposal ID: MA6644
beamline: ID16BÂ
Understanding early age low carbon cement hydration acceleration by in-situ nanotomography
ALBA June 25:Â
10/06/2025 - 13/06/2025
proposal ID: 2024098574Â
beamline: BL31 - FaXToRÂ
Understanding hydration acceleration of Limestone Calcined Clay Cements at early ages by in-situ X-ray tomography