Paper Review

Paper Review


S. GOYA a, H. MORI b, T. OKUDA b , Y. FUJIYA c, N. SHIMONABE d, T. AKABA e

a)Research Manager, Manufacturing Technology Research Department, Research & Innovation Center, Mitsubishi Heavy Industries, Ltd. 

b)Manufacturing Technology Research Department, Research & Innovation Center, Mitsubishi Heavy Industries, Ltd. 

c)Senior Manager, Manufacturing Technology Research Department, Research & Innovation Center, Mitsubishi Heavy Industries, Ltd. 

d)Chief Staff Manager, Nuclear Plant Component Designing Department, Nuclear Energy Systems, Mitsubishi Heavy Industries, Ltd. 

e)Manager, Research & Development Department, Nuclear Plant Service Engineering Co., Ltd. 


With the increasing power and better quality of laser oscillators, laser processing, which has not been applied to thick concrete, has been increasingly used in recent years. In this report, we describe laser cutting of thick concrete columns (with a maximum thickness of 1200 mm) by using high-power fiber laser of over 20 kW and an ultra-long focus optical system, aiming at establishing a remote demolition technology for nuclear plant buildings that are high radiation areas. This report also describes a new beam laser damper system using water that was developed as a technology for receiving the high-power laser beam passing through a cutting object, which has been an issue in high-power laser processing. 

M. Domke a, V. Matylitsky b, S. Stroj a 

a)Josef Ressel Center for Material Processing with Ultrashort Pulsed Lasers, Research, Center for Microtechnology, Vorarlberg University of Applied Sciences, Hochschulstr. 1, Dornbirn 6850, Austria 

b)Spectra-Physics, Feldgut 9, Rankweil 6830, Austria 


In recent years, the burst-mode caught a lot of attention in the field of ultrashort-pulse laser micro machining. One of the major issues is the influence of the burst pulse number and frequency on ablation efficiency and quality. A recent publication reported of a significant increase in ablation efficiency when processing with ≥25 burst pulses at ≥100 MHz burst frequencies. This raises the question of whether processing with such high pulse densities can be attributed to non-thermal ablation, or whether a quasi-nanosecond laser ablation behavior is achieved. To answer this question, we determined ablation efficiencies as function of fluence for silicon, stainless steel, and copper and compared the ablation quality at the optimal fluence using the following laser systems: femtosecond laser operated in single-pulse mode, fs laser operated in 28-pulse-burst mode with a burst pulse frequency of 148 MHz, and a nanosecond laser with a pulse duration of 175 ns, which is identical with the temporal length of the burst pulse train. The comparison showed that the burst mode used produces similar surface morphologies and melt burrs as the nanosecond laser, but at about 2/3 of its efficiency. 

Menglei Zhao a, Zeng Yang a, Jingnan Zhao a b, Pranav Shrotriya a b c, Yan Wang a b, Yuanchen Cui d, Zhiquan Guo a b 

a)Tianjin University of Science and Technology, Tianjin, China

b)Tianjin Key Laboratory of Integrated Design and On-line Monitoring for Light Industry & Food Machinery and Equipment, Tianjin, China

c)Iowa State University, Department of Mechanical Engineering, Ames, USA

d)U. S. Polyco, Ennis, USA


In this paper, a hybrid ultrasonic vibration assisted laser (UVAL) prepared copper surface of super-hydrophobic was reported. After UVAL treatment, the water contact angle (WCA) of copper surface to 3 μL water was 157.4°and the water slip angle (WSA) was less than 10°. The wettability, microstructure, chemical composition and durability of copper surface were measured by contact angle measuring instrument, field emission scanning electron microscopy (FESEM), surface predatory X-ray diffraction (XRD) and three-dimensional morphology. The results revealed that after UVAL treatment, the microcoral-like structure and nano-grass structure were formed on the surface of the sample, which were similar to the surface of lotus leaf. Ultrasonic vibration combined with laser treatment can accelerate the adsorption of airborne hydrocarbon contaminations on the surface of micro and nanostructures, and reduce the surface energy of copper particles on the surface. This study provides a fast, convenient and effective method for the rapid preparation of stable superhydrophobic copper surface. 

A. Anthofer*, W. Lipopmann and A. Hurtado

Chari of Hydrogen and Nuclear Engineering, Institute of Power Engineering, Technische Universitaet Dresden, Germany


Decontamination of radioactive concrete surfaces may be necessary during operation or decommissioning of nuclear power plants. Usually only the upper layers of the concrete structure are contaminated and are removed using labor-intensive mechanical milling processes. Production of a large amount of dust, which can lead to secondary contamination, is inherent to these processes. Improvements in high-energy laser technology have now made it possible for laser radiation to be used in decontamination technologies for the removal of concrete layers. A decontamination unit comprising a diode laser with a beam power of 10 kW in continuous wave (CW) mode in combination with an autonomous manipulator was developed for use in nuclear plants. The laser beam melts the concrete surface to a depth of approximately 5 mm. Compressed air jets then detach the molten layer from the concrete surface and convey it to a suction system, with which it is transported to a collection container. Most of the radionuclides are trapped in the solidifying melt particles, which form an extremely stable effluent well suited to long-term storage. A relatively small amount of dust is generated in the process. Because there is no backlash during energy transfer, the laser device carrier can be designed to be lightweight and flexible. A specially developed manipulator that can move freely along walls and ceilings by means of suction plates is used for the carrier unit. This results in short setup times for preparing for use of the device and minimal personnel exposure to the radiation. Experiments were conducted on a concrete wall to demonstrate the functionality of the overall system in realistic conditions. An optimal ablation rate of 2.16 m2 /h at an ablation depth of 1–5 mm was achieved. Today’s commercially available diode lasers with powers higher than 50 kW enable ablation rates of 410 m2 /h to be achieved and hence make these laser-based systems competitive alternatives to mechanical systems.

H. Kariminezhad1) , H. Amani2) and M. Moosapoor1)

1)Department of Physics, Babol University of Technology, Babol, Iran

2)Faculty of Chemical Engineering, Babol University of Technology, Babol, Iran


Laser perforation is the application of light to make a flow path between wellbore regions through the casing wall and cement layer all the way to reservoir production zone. Due to significant losses of laser power at long distances, introducing a novel method in order to facilitate laser perforation in oil and gas reservoirs is necessary. This paper aims to study on concrete perforation using a continuous 240 W/cm2 CO2 laser. In this research, the effect of water on the parameters of laser perforation such as rate of perforation (ROP), specific energy (SE) and dominant mechanisms was investigated. For this, two groups of concrete samples (dry and wet) were illuminated at 2, 6, 15, 30 and 60 s by the laser. Our results showed evaporation was main mechanism for dry samples at exposure times above 15 s, while spallation was the dominant mechanism for the wet samples at all exposure times. ROP and SE were significantly increased and decreased in the presence of moisture, respectively. Maximum ROPs obtained 2.26 mm/s and 0.45 mm/s for wet and dry samples, respectively. Also, minimum of SEs for wet and dry samples obtained 1.05 J/mm3 and 4.3 J/mm3, respectively. Finally, our experimental results were justified using a simplified heat conduction model. All these characteristics demonstrate presence of water in concrete possesses an important role to improve rate of laser perforation. Therefore, the results of this research could significantly reduce time and cost of laser perforation for application of oil recovery. 

K. Nagai1) and K. Shimizu1)

1)Department of Architecture and Architectural Engineering, College of Industrial Technology, Nihon University, Japan


Concrete cutting at construction sites causes problems such as noise, vibration, and dust. In particular, during the demolition and renovation work on buildings in urban areas, protection against noise, vibration, dust, etc., is needed. Concrete cutting using a CO2 laser was investigated 20 years ago. However, this method had never used because the equipment is difficult to carry. In this study, we used a portable fibre laser, which is convenient to carry. Two types of concretes with different strengths were prepared for the experiment. High-strength concrete has never been used in similar research before. High-strength concrete is just only used for skyscrapers because of its high quality and cost. Furthermore, it has already been used for skyscrapers in Japan. It is for this reason that we chose to use it in this study. Irradiation measurements were conducted under various conditions using laser powers of 6 and 9 kW. It was confirmed that the cutting effectiveness of CO2 and fibre las ers was approximately identical for concretes with a thickness of 200 mm. Furthermore, the cutting effectiveness for the two concretes with different densities was almost the same. However, the situation after cutting was different because the vitrification of the cutting and glass formation progressed in low-density concrete and an explosion phenomenon occurred in high-density concrete, simultaneously. This study suggests that laser concrete cutting can be used as a solution when noise and dust are major problems. 

31. Laser weldability of cast and rolled high-entropy alloys for cryogenic applications

H. Nam1), C. Park1), J. Moon3), Y. Na2), H. Kim3), and N. Kang1)

1)Department of Materials Science and Engineering, Pusan National University, Republic of Korea

2)Titanium Department, Korea Institute of Materials Science, Republic of Korea

3)Department of Materials Science and Engineering, Pusan UniversityNational University, Republic of Korea


Laser similar welding of cast and rolled high-entropy alloys (HEAs) was performed using the cantor system (Co0.2Cr0.2Fe0.2Mn0.2Ni0.2). As the welding velocity was increased from 6 to 10 m min−1, the shrinkage voids, primary dendrite arm spacing, and dendrite packet size decreased, thus improving the mechanical properties of the cast and rolled HEA welds. The cast HEA welds showed tensile properties comparable to those of the base metal (BM). In all the specimens fracture occurred near the heat-affected zone and BM at 298 K. However, the rolled HEA welds showed lower tensile strength than the BM, and fracture occurred in the weld metal (WM). This can be attributed to the larger dendrite packet size of the WM than the grain size of the BM. In addition, the tensile properties of the specimens at the cryogenic temperature were superior to those observed at 298 K, regardless of the cast and rolled HEA welds. This is because the formation of deformation twins and dislocations was predominant at 77 K. Therefore, the laser similar welds of cast and rolled HEAs are suitable for cryogenic applications. 

J. Chen1), J. Zhang1), K. Li2), D. Zhuang2), Q. Zang3), H. Chen3), Y. Lu4), B. Xu4) and Y. Zhang1)

1)School of metallurgy and materials engineering, Jiangsu University of Science and Technology, China

2)School of materials science and technology, Jiangsu University, China

3)School of materials science and technology, Jiangsu University of Science and Technology, China

4)Suzhou institute of technology, Jiangsu University of Science and Technology

In this study, laser surface remelting of an AlCoCrFeNi2.1 high-entropy alloy was performed using a Yb:YAG laser. The effects of laser surface remelting on the phase structure, microstructure, Vickers hardness, frictional wear properties, and corrosion resistance of the high-entropy alloy were investigated. The remelted layer of the AlCoCrFeNi2.1 high-entropy alloy was produced by remelting at 750 W laser power and formed a good metallurgical bond with the substrate. The X-ray diffraction results showed that the 750 W remelted layer consisted of face-centered cubic and body-centered cubic phases, which were consistent with the phases of the as-cast AlCoCrFeNi2.1 high-entropy alloy, and a new phase was not generated within the remelted layer. Laser surface remelting is very effective in refining the lamellar structure, and the 750 W remelted layer shows a finer lamellar structure compared to the matrix. The surface hardness and wear resistance of the AlCoCrFeNi2.1 high-entropy alloy were substantially improved after laser surface remelting. In a 3.5 wt.% NaCl solution, the laser-remelted surface had a larger self-corrosion potential and smaller self-corrosion current density, and the corrosion resistance was better than that of the as-cast high-entropy alloy. 

A. Y. Vorobyev1) and  C. Guo1)

1)The institute of optics, University of Rochester, USA

This research team has demonstrated, visually and through spectral measurements, the creation of color metals with femtosecond laser surface structuring technique. We show that our technique essentially provides a controllable modification of optical properties of metals from UV to terahertz via surface structuring on the nano-, micro-, and submillimeter-length scales. The size of the optically modified metal surface area can be as small as a tightly focused laser spot, i.e., down to about 10 m, or as large as needed when a scanning laser beam is used. Given the additional advantages of laser processing such as low contamination and the capability to process complicated shapes, the color metals created in this work have tremendous potential in various technological applications. 

Seong Y. Oh1), Gwon Lim1), Sungmo Nam1), Byung-Seon Choi1)

1)Korea Atomic Energy Research Institute

The experimental study is conducted to investigate the effect of silica fume mixed in concrete blocks on laser-induced explosion behavior. We use a 5 kW fiber laser as a thermal source to induce explosive spalling on a concrete surface blended with and without silica fume. An analytical approach based on the difference in the removal rate and thermal behavior is used to determine the effect of silica fume on laser-induced explosive spalling. A scanner is employed to calculate the laser-scabbled volume of the concrete surface to derive the removal rate. The removal rate of the concrete mixed with silica fume is higher than that of without silica fume. Thermal images acquired while scabbling is used to qualitatively analyze the thermal response of laser-induced explosive spalling on the concrete surface. At the early stage of laser heating, an uneven spatial distribution of surface temperature appears on the concrete, including silica fume, because of frequent explosive spalling within a small area. By contrast, in laser-heated concrete without silica fume, the spalling frequency is relatively lower, and a larger area is removed via one explosive spalling event owing to its high porosity. 

K. Huehnlein 1), K. Tschirpke 1), R. Hellmann 1)

1)University of Applied Science Aschaffenburg, Wuerzburger Strasse 45, D-63743 Aschaffenburg Germany  

Basem F. Yousef 1) ,George K. Knopf 1), Evgueni V. Bordatchev 2), Suwas K. Nikumb 2) 

1)Department of Mechanical and Materials Engineering, The University of Western Ontario, London, N6A 5B9, Canada  

2)Integrated Manufacturing Technologies Institute, National Research Council of Canada, London, Canada 

Youmin Rong1), 2) ,Yu Haung1), 2) ,Congyi Wu1), 2) 

1)Kstate Key Lab of Digital Manufacturing Equipment and Technology, Huazhong University of Science and Technology, Wuhan, China 

2)Kschool of Mechanical Science and Engineering, Huazhong University of Science and Technology, Wuhan, China

Paul Hilton(1), Colin Walters(1)

(1) TWI Ltd, Granta Park, Great Abington, Cambridge CB21 6AL, UK

J.L. Song(1,2*), Y.T. Li(1), Q.L. Deng(2), D.J. Hu(2)

(1) School of Materials Science and Engineering Taiyuan University of Science & Technology, Taiyuan 030024, China

(2) School of Mechanical and Power Engineering, Shanghai Jiaotong University, Shanghai 200030, China

S. Stoyanov, D. Petring, D. Arntz, M.Gunder (1), A. Gilner, R. Poprawe (2)

(1)Fraunhofer Institute for Laser Technology, Steinbachstr. 15, 52074 Aachen, Germany

(2)Chair for Laser Technology LLT, RWTH Aachen University, Steinbachstr. 15, 52074 Aachen, Germany

Chongjing Hu, Gaoyang Mi, Chunming Wang (1)

(1) State Key Laboratory of Material Processing and Die & Mould Technology, Huazhong University of Science and Technology, Wuhan, Hubei 430074, China

Joerg Volpp (1)

(1) Department of Engineering Sciences and Mathematics, Lulea University of Technology, Lulea, Sweden 

A. Jung (1), H. George (1), Florian Kiefer (1)

(1) TRUMF Inc., 47711 Clipper Street Plymouth Township 48170 Michigan, United States of America

Meng Jiang(1, 2), Xi Chen(1), Yanbin Chen(1), Wang Tao(1), Tarasankar DebRoy(2)

(1) State Key Laboratory of Advanced Welding and Joining, Harbin Institute of Technology Harbin, 150001, China 

(2) The Department of Materials Science and Engineering, The Pennsylvania State University Park, PA, 16802, U.S.A 


17. Laser decontamination of epoxy painted concrete surfaces in nuclear plants

원전 내 에폭시 도색 콘크리트 표면의 레이저 제염

A. Anthofer, W. Lippmann, A. Hurtado

https://www.sciencedirect.com/science/article/pii/S0030399213003599 

Laser technology offers an efficient decontamination of surfaces contaminated by polychlorinated biphenyls (PCB) by precise application of highly focused laser beam power. In the context of nuclear decommissioning all walls and floors of a reactor building have to be cleaned from chemical-toxic substances. State of the art is a manual and mechanic ablation and a subsequent treatment in a hazardous waste incinerator. In this study, alternatively, a laser-based system exhibiting, decontamination rates of up to 6.4 m^2/h has been operated using a 10-kW diode laser in continuous wave (CW)mode with a spot size of 45 X 10 mm^2 and a wavelength of 980–1030 nm. The system allows a rapid heating of the surfaces up to temperatures of more than 1000 celsius degree leading to ablation and thermal decomposition of PCB  in one process step. Thermal quenching prevents formation of polychlorinated dioxines (PCDD) and polychlorinate furans (PCDF) in the flue gas. Additionally, an in situ measurement system based on laser induced fluorescence (LIF) is developed to monitor the thermal decomposition of PCB. Forinitial experiments samples covered with epoxy paint were used to evaluate the process and to carry out finite element based simulations. In this paper, experimental results of ablation tests by laser irradiation of epoxy painted concrete are presented and discussed.


16. Ultra-high power (100kW) fiber laser welding of steel

철의 초-고출력 (100kW) 파이버 레이저 용접

YOUSUKE KAWAHITO, HONGZE WANG, SEIJI KATAYAMA, AND DAICHI SUMIMORI

https://www.osapublishing.org/ol/abstract.cfm?uri=ol-43-19-4667 

    A 100 kW fiber laser was first used to weld steel. Speeds at the range between 0.3 and 5.0 m/min were tested, and the maximum weld bead depth of 70 mm was achieved by single pass welding. Solidification cracking and porosity occurred when the welding speed was lower than 0.5 m/min, while undercut appeared when the welding speed was higher than 3.0 m/min. Both the ratio of depth to width and the cross section area of the weld bead had a positively linear relationship with the welding speed. A high speed camera was used to observe the characteristics of the keyhole and molten pool. The average number of spatters increased with the welding speed, while the keyhole diameter and the length of the molten pool in front of the keyhole decreased with the welding speed. This Letter validates the application potential of a 100 kW ultra high power fiber laser in manufacturing, e.g., welding, cutting, and additive manufacturing.

15. Studies on enhanced thermally stable high strength concrete incorporating silica nanoparticles

실리카 나노입자가 함유된 열안전성이 향상된 고강도 콘크리트에 관한 연구

R. Kumar, S. Singh*, L.P. Singh

https://www.sciencedirect.com/science/article/pii/S0950061817313934

 The performance of silica nanoparticles incorporated high strength concrete (SNPs-HSC) has been evaluated under elevated temperature conditions by exposing up to 800  C, followed by cooling to ambient temperature before performing experiments. Time-temperature studies revealed that incorporation of silica nanoparticles (SNPs) in concrete mix delays the heat transfer by 11%, 18%, 22% and 15% at 200  C, 400  C, 600  C and 800  C respectively thereby, decreasing the rate of degradation as compared to the conventional high strength concrete (HSC). A reduction in weight loss was observed in SNPs- HSC specimens after exposure to 200  C, 600  C, and 800  C; whereas at 400  C the weight loss quantity was  3.5% higher than the control HSC specimens due to the evaporation of water from calcium silicate hydrate (C-S-H) gel. On exposure up to 400  C for 2 h, the compressive strength and split-tensile strength increased by 40% and 13% respectively, for SNPs-HSC specimens, whereas in control HSC specimen’s strength didn’t increase after 200  C. A higher residual compressive (7%) and split-tensile strength (8%) was found to be in SNPs-HSC specimens exposed to 800  C for 2 h as compared to the control HSC specimens. The stress-strain curves revealed that SNPs-HSC specimens exhibits brittle failure up to 600  C whereas in control HSC brittle failure was observed only up to 400  C. Microstructural studies performed on the samples taken from the core of the 400  C exposed SNPs-HSC revealed the formation of higher C-S-H content and lower amount of calcium hydroxide (CH) leading to their enhanced mechanical and thermal stability. 


14. Laser scabbling of mortars

모르타르의 레이저저 스케블링

B. Peach*, M. Petkovski*, J. Blackburn, D.L. Engelberg

https://www.sciencedirect.com/science/article/pii/S0950061816311382

Laser scabbling of concrete is the process by which the surface layer of concrete may be removed through the use of a low power density laser beam. Previous research has suggested that the driving force responsible for laser scabbling is developed within the mortar. The aim of this investigation was to establish the key parameters that influence laser scabbling of mortars. All scabbling tests were carried out using an IPG photonics YLS-5000 (5kW) Yb-fibre laser. the specimens were subjected to a static, continuous, diverging laser beam with a stand off distance of 340mm from the focal point which gave a nominal beam diameter of 50mm. Tests were conducted with the laser beam applied to a vertical concrete surface to avoid debris falling back onto the specimen during testing. The results show that the removal of free water from mortars prohibits scabbling, but resaturation allows mortar to scabble. A reduced permeability, either due to a reduction in the water/binder ratio or the use of 25% PFA replacement, enhances the scabbling. A higher fine aggregate content increases volume removal and fragment sizes during laser scabbling.


13. Laser cutting of aluminium-alumina metal matrix composite

알루미늄-알루미나 금속 메트릭스 복합체의 레이저 절단

S. Marimuthu, J. Dunleavey, Y. Liu, M. Antar, B. Smith

https://www.sciencedirect.com/science/article/pii/S0030399219302506?via%3Dihub

Laser cutting of monolithic materials like metals and alloys is well-established and is used extensively in various industries including aerospace, medical and automotive. However, laser cutting of anisotropic materials like metal matrix composites (MMC) is challenging due to the differences in the chemical and physical properties of the matrix and fibre reinforcement. This manuscript contains details and results of an investigation into laser cutting of 2mm thick aluminium metal matrix reinforced with aluminium oxide fibre (Al MMC). The laser cutting mechanism and the influence of laser cutting parameters on the quality of cuts were examined in detail. The experimental results demonstrated that the laser cutting mechanisms of fibre reinforced MMCs are vastly different from the mechanisms observed in laser cutting of monolithic metals and alloys. The Al2O3 fibres within the MMC are not vaporized but are removed along with the molten, low melting point matrix materials. A thin and uniform layer of Al2O3 was been deposited over the cut surface which can be advantageous for applications that involve moving gases or fluids, for example, aero-engine cooling holes.

12. Surface Cleaning of Metals Using Low Power Fiber Laser

저출력 fiber laser를 이용한 금속 표면 세정

E. KAYAHAN, L. CANDAN, M.ARAS and O. GUNDOGDU


Lasers are used in industry in a large variety of applications. These applications can mainly be divided into two categories: one specifically being materials processing. Material processing includes cutting, drilling, welding, etc., and generally involves the use of high-powered lasers. Laser applications such as rust/dye removal and surface cleaning are not yet very common for the industry. This paper reports experiments on industrial applications of a ytterbium fiber laser (1064 nm) with a maximum output power of 20 W, pulse duration of 200 ns and pulse repetition rate of 10-100 kHz. Furthermore, the laser beam was focused on the target through a 160 mm focal length F-T lens. Scanning speed and line spacing of laser are 3-100 mm/s and 1-100 um, respectively. Experimental studies showed that a low-power fiber laser could be used for a variety of applications such as surface cleaning of metals and rust-dye removal. Optimum laser parameters were also determined for these applications.


11. High-Power Fibre Laser Cleaning for Green Shipbuilding

 G. X. Chen, T. J. Kwee, K. P. Tan, Y. S. Choo and M. H. Hong


Blasting techniques in shipbuilding and ship repair have been developed for surface preparation of steel to a standard equivalent to SA2.5 as defined by ISO Standard 8501. The usage of consuma-bles, such as abrasive materials, air and water, constitutes a recurring cost in these processes. When blasting work is carried out in the open space, such as during a dry docking, abrasive blasting gen-erates a lot of dusts which in turn pollutes the environment with consequential social and economi-cal costs. Laser blasting or laser cleaning, which has not been introduced commercially in shipbuild-ing and ship repair, offers an alternative for green manufacturing and green repairs. Laser cleaning has significant advantages on these issues over the conventional blasting techniques. It is a well-controlled process with unique properties, such as precise treatment, high selectivity, and high flexi-bility. A cleaning technique using a high-power fibre laser is developed for the surface preparation of steel. Fibre laser has advantages of compact system, automation capability, and low maintenance cost. We report the laser cleaning results using a 500-W pulsed high-power fibre laser. The laser cleaning is able to meet the SA 2.5 requirements of blast cleaning as described in the International Organization for Standardization (ISO) standard 8501.


10. Microstructural analysis of interfacial transition zone (ITZ) and its impact on the compressive strength of lightweight concretes

Interfacial transition zone (ITZ)의 미세 구조 해석과 경량 콘크리트의 압축강도에 미치는 영향 

P. Vargas, Oscar Restrepo-Baena, Jorge I. Tobón

https://www.sciencedirect.com/science/article/abs/pii/S0950061817301320?via%3Dihub

This study observed the microstructure and thickness of the interfacial transition zone (ITZ) in concretes of Portland cement and lightweight aggregates (LWA). It has been established that the microstructure in the ITZ strongly depends on the nature of the aggregate, specifically its porosity and water absorption. This study aims at researching the influence of physical properties such as density, porosity and morphology of lightweight aggregates such as pumice and expanded clays, on the microstructure and thickness of ITZ, and determine the effect that these factors have in turn on the mechanical properties as compressive strength of lightweight concretes (LWC). Lightweight aggregates were characterized by X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and X-ray Fluorescence (XRF), to determine their mineralogical, morphological and chemical characteristics. The characterization of ITZ by SEM-EDS, and conventional optical microscopy, was carried out on specimens of concrete manufactured with LWA and with a conventional aggregate, in order to evaluate its thickness; furthermore, to determine the porosity, digital image processing (DIP) was performed. Lightweight aggregates contributed to the formation of a dense and thinner ITZ, when compare to the ITZ of a conventional concrete. The lower porosity and greater amount of hydrated cement phases in the ITZ of lightweight aggregates are attributed to their physical, morphological properties and chemical and mineralogical composition; which contributed to the decrease of the wall effect, gestating from its surface the formation of C-S-H, achieving interlacing of hydrated phases on the surface of these aggregates with the cementitious matrix.


9. Determination of dissipated Energy in Fatigue Crack Propagation Experiments with Lock-In Thermography and Heat Flow Measurement

Lock-In Thermography와 Heat Flow 측정을 이용한 피로 균열 진전 실험에서 소산 에너지의 결정

Jurgen Bar

https://www.sciencedirect.com/science/article/pii/S245232161630275X

   Lock-in thermography and heat flow measurements with peltier sensor(TEC-1089-SV) was performed during fatigue crack growth testing. Moreover, elastic stress fields (E-Amplitude) as well as dissipated energies (D-Amplitude) can be determined. In case of thermographic measurements the specimens have to be painted to enhance the emissivity, but the thickness of the coating influences the results and therefore quantitative measurements are problematic. The heat flow measurements are easy to perform and provide quantitative results, but only integral values in an area given by the size of the peltier element can be achieved. In order to get comparable results the evaluation of the thermographic measurements were performed in the same area as the peltier measurements. In case of the mean temperature measured by thermography and the heat flow determined with the peltier sensor a good agreement was found. The measurement of elastic stresses with the peltier sensor is restricted to low loading frequencies due to the response characteristic of the sensor. For the measurement of dissipated energies the cooling of the specimen by heat conduction into the clamps and heat radiation has to be taken into account.


8. Investigation on rock breaking for sandstone with high power density laser beam

고출력 레이저 빔을 이용한 사암 암석 파괴에 대한 조사

Meiyan Li, Bin Han, Qi Zhang, Shiyi Zhang, Qingkun He


https://www.sciencedirect.com/science/article/pii/S0030402618315584?via%3Dihub

   High power density laser was applied during rock breaking for sandstone with different laser parameters. The fracture morphology and quantitative characterization as well as the parameters on specific energy and rate of perforation were analyzed. It was found that a complex crack net structure was formed and the cracks area and length on the surface of sandstone specimen almost increased linearly with the number of laser perforation. Furthermore, the diameter and depth of laser perforation, the maximum width of cracks, the maximum depth and total circumferential length of side cracks increased with laser power and laser irradiation time. The experimental results demonstrated that the SE values gradually decreased with laser power while the ROP values increased. However, the SE values of sandstone by laser perforation presented a trend of first increase and then decrease, while the ROP values decreased gradually with laser irradiation time. A smooth glaze layer was formed on the inner wall of the laser perforation, where there also was plenty of shrinkage hole. Obvious cracks were generated and propagated along the inner wall. Typical brittle fracture occurred with the mix fracture mechanisms of intergranular fracture and transgranular fracture.


7. Advanced rock drilling technologies using high laser power

고출력 레이저를 사용하는 응용 암반 천공 기술

Frederik Buckstegge, Theresa Michel, Maik Zimmermann, Stephan Roth, Michael Schmidt


https://www.sciencedirect.com/science/article/pii/S1875389216301420

  Conventional drilling method on hard rock formations causes high mechanical wear and most often environmental disturbance. This study focuses on the interaction of laser irradiation with calcite, porphyrite and siderite rock formations. The irradiation tests were performed using a fiber coupled disc laser. The high-power disc laser system at 1030nm wavelength was used to investigate the specific energy necessary to remove a unit volume depending on interaction times and applied power. The samples studied were five samples of rocks. Specific energies have been measured and an increase of fragility and brittleness of the rock surface has been observed.

6. Experimental Investigation of Multi-mode Fiber Laser Cutting Cement Mortar

다중 모드 광섬유 절단 시멘트 모르타르의 실험적 연구

D. K. Lee, S. H. Pyo


https://www.mdpi.com/1996-1944/11/2/278

    건설사업에서 콘크리트 구조물의 열화된 부분을 제거하기 위해 레이저 조사 기술을 적용할 수 있다. 따라서, 이 연구는 시멘트 복합재료의 레이저 절단에 초점을 두고 진행하였다. Multi-mode fiber laser는 레이저 빔 직경 100 um, 레이저 파워 1000 W를 사용하며 N2 보조 가스는 7 bar로 실험 설정하였다. 또한, scanning speed를 매개변수로 설정하고 이를 통해 단위 면적당 조사된 에너지 양인 Line energy를 나타내었다. 실험에 사용된 cement-based materials는 물과 시멘트 비율, silica sand, silica powder, silica fume의 양을 변수로 설정하여 제작하였다. 실험 결과로는 kerf width와 penetration depth를 측정하여 평가하였다. 또한, 레이저 절단 영역에서 화학적 변화를 평가하기 위해 EDS 성분분석을 진행하였다. 본 연구를 통해 cement-based material에 silica sand를 혼합하면 kerf width와 penetration depth가 감소함을 확인하였으며 절단 영역에서 화학적 조성의 변화가 수산화칼슘의 탈수 및 탄산 칼슘의 분해를 비롯한 다양한 메커니즘에 의해 야기된다는 것을 확인하였다.

5. SEM investigation of microstructures in hydration products of portland cement

포틀랜드 시멘트의 수화 생성물에 대한 미세구조의 SEM 조사

W. Franus, R. Panek, M. Wdowin


https://docplayer.net/21502550-Sem-investigation-of-microstructures-in-hydration-products-of-portland-cement.html

     포틀랜드 시멘트는 콘크리트 복합재를 포함한 많은 건축 자재의 제조에서 주요 성분 중 하나이다. 연구에 사용된 재료는 Portland cement CEM Ⅰ 42.5 R(450g), standard sand (1350g), water(225g)이며 이와 같이 형성된 시편을 28일에서 90일까지 숙성하였다. 수화 생성물의 상 조성은 XRD 및 DTA/TG 분석을 통해 관찰하고 시멘트 페이스트의 상 변화 및 미세구조를 SEM/EDS 분석을 통해 관찰하였다. 시멘트 수화 단계는 크게 3가지로 물과 시멘트를 혼합한 뒤, 시간에 따라 분류된다. 첫 번째 단계에서는 수산화칼슘(Portlandite)이 분리되며 이는 Tri-calcium silicate와 di-calcium silicate의 가수분해를 통해 형성된다. 또한, 포틀랜드 시멘트의 페이스트에서 최대 부피 25%의 고체상이 형성된다(Fig.1). 두 번째 단계에서는 C-S-H(Calcium-Silicate-Hydration)가 생성된다. 이 때 포틀랜드 시멘트의 페이스트에서 최대 부피 50~60%의 고체상이 형성되며 페이스트에서 특징적인 형태가 없는 수화 생성물들이 관찰된다(Fig.2). 세 번째 단계에서는 C-S-H의 짧은 섬유 또는 층상구조에 의해 공극(porosity) 충진이 발생한다. 포틀랜드 시멘트의 페이스트에서 완전히 고체상이 형성되며, Ettringite 결정은 침주상이고 tobermorite는 층상 형태로 관찰된다(Fig.3). SEM/EDS를 통해 시멘트 페이스트 또는 콘크리트의 미세구조 물리적 및 화학적 변화를 관찰할 수 있으며(Fig. 4), 시멘트 페이스트 수화 과정에서 발생하는 주상의 형태의 변화를 바탕으로 시멘트 모르타르 및 콘크리트의 특성을 예측하는 것이 가능하다. 

Fig.1 Hexagonal plate of portlandite

Fig.2 C-S-H and plate of portlandite

Fig.3 Needle crystals of ettringite

EDS of C-S-H phase

EDS of portlandite

EDS of C-S-H honeycomb 

Fig.4 Mineral phases occurring in maturing cement paste

4. The effects of process gas type on the surface condition of high-power diode laser-treated ordinary Portland cement

고출력 다이오드 레이저 처리된 일반 포틀랜드 시멘트의 표면 상태에 대한 공정 가스 유형의 영향

J. Lawrence*, L. Li


https://www.sciencedirect.com/science/article/pii/S0143816601000641

     고출력 다이오드 레이저 (HPDL)를 사용하여 일반 포틀랜드 시멘트 (OPC) 표면 처리시 O2, Ar 및 He 공정 가스 사용의 효과에 대해 관찰하였다. 실험에 사용된 시편은 Ubiquitous OPC 기반 콘크리트(120 x 120 x 20 )이며 레이저는 최대 출력 120W, 파장 810nm에서 HDPL(Diomed Ltd.)를 사용하였다. HDPL 빔은 길이 4m, 코어 직경 1mm의 광섬유를 사용하였고 연속파(CW)모드에서 작동하고 다중 모드 빔을 생성하였다. CNC 테이블의 x축, y축으로 작동하여 60~600 mm/min의 속도로 실험하였다. 또한, 서로 다른 차폐 가스의 효과를 연구하기 위해 , Ar 및 He의 가스를 분사하였다. 연구 결과, 사용된 차폐 가스에 따라 HPDL 처리 후 콘크리트의 표면 상태에 뚜렷한 차이가 있음이 밝혀졌습니다. 특히, 실드 가스로서의 O2의 사용은 Ar 또는 He 실드 가스로 생성된 것보다 훨씬 적은 미세 균열 및 다공성을 갖는 유약을 생성하는 것으로 나타났다(Fig.1). 이러한 차이는 콘크리트의 OPC 표면에서 HPDL이 생성된 유약의 분자 구조로 분자 적으로 용해되는 보다 작은 O2 가스 분자가 유리 망과 반응하여 용융물의 유동성을 증가시키는 것으로 나타났다. 이것은 또한 냉각 속도 및 미세 균열을 발생시키는 경향에 영향을 받는다(Fig.2).

Fig.1 Typical optical surface morphology of the HPDL treated OPC surface with (a) O2, (b) Ar and (c) He shield gas.

Fig.2 Best-fit cooling rate curves for the laser-glazed OPC surface of concrete when O2, Ar and He shield gases were employed.

3. Microstructure evolution and mechanical characterization of Nd:YAG laser beam welded titanium tubes

Nd:YAG 레이저 빔 용접 티타늄 튜브의 미세 구조 진화와 기계적 특성

R. Palanivel⁎, I. Dinaharan, R.F. Laubscher


https://www.sciencedirect.com/science/article/pii/S1044580317324786

     외경 60 mm 및 두께 3.9 mm의 2 등급 티타늄 튜브는 Nd : YAG 레이저(4.4 kW Rofin Sinar DY 044)로 효과적으로 결합되었다(Fig.1). 레이저 파워는 4kW이며 용접 속도는 2.50m/min부터 3.50m/min까지 0.25m/min 간격으로 다양하게 실험하였다. 미세 구조 진화는 광학 현미경 및 고급 특성화(FESEM, EDAX, EBSD, XRD) 기술을 사용하여 연구하였다. 비드 형상은 평행 형상에서 쐐기 형상으로 변경되며, 표면 장력의 변화로 인해 용접 속도가 증가한다(Fig.2). 레이저 처리된 영역에서 Fusion Zone, Heat Affected Zone (HAZ) 및 Base Metal과 같은 세 영역이 관찰되었다(Fig.3). Fusion Zone에서는 불규칙하고 톱니 모양의 거친 입상 구조가 관찰되었다. 구형 및 불규칙한 형태의 pores(기공)은 낮은 용접 속도일 때 Fusion Zone의 중앙선 근처에서 관찰되었다. 이는 고형화가 되면서 내부에 갇힌 가스로 인해 발생되었다. 결정립 크기는 냉각 속도가 높아짐에 따라 용접 속도가 증가할수록 감소하였다. 또한, 응고에 의한 열 응력으로 인해 용융 영역에서 높은 밀도의 전위가 관찰되었다. Fusion Zone의 미세 경도는 하부 구조 경계, 용질 요소 및 전위로 인해 레이저 처리 전의 금속보다 높게 관찰되었다. 용접 속도가 증가함에 따라 Fusion Zone에서 기본 금속으로의 파단 위치가 바뀌고 부서지기 쉬운 상태에서 연성 모드로 변경되었다.

Fig.1 Laser beam welding set up 

Fig.2 Optical macrographs of welded joints at a welding speed of; (a) 2.50 m/min, (b) 2.75 m/min, (c) 3.00 m/min (d) 3.25 m/min and (e) 3.50 m/min.

Fig.3 Optical and EBSD images of a weld joint at a welding speed of 3.25 m/min. a) The cross sectional micrograph of the transition zone b) change in crystallographic orientation due to the welding.

2. Performance comparison of CO2 and diode lasers for deep- section concrete cutting

Deep-section 콘크리트 절단을 위한 CO2 및 다이오드 레이저의 성능 비교

Philip L. Crousea, Lin Li,*, Julian T. Spencer


https://www.sciencedirect.com/science/article/pii/S0040609003017486

     Layer-by-layer laser machining with mechanical removal of vitrified dross between passes is a new technique with a demonstrated capability for deep-section cutting, not only of concrete, but of ceramic and refractory materials in general. The experiments were performed using a Rofin-Sinar RS-1000 1.2kW, fast axial flow CO2 laser, and a laser line LDL-160-1500 1.5 kW high-power diode laser. Furthermore, In the experiments reported here 150, 150, and 45 mm3 as received concrete slabs, manufactured from Portland cement and limestone aggregate, were used as work pieces. A comparison of experimental results using the CO2 laser and high-power diode lasers under roughly equivalent experimental conditions cutting to depths of >100 mm, is described. As a result, a concrete cutting technique based on a high-powered diode laser rather than a CO2 is the better choice. The rectangular beam shape of the diode laser affords a wider and more parallel kerf, extremely important for deep-section concrete cutting. Also, the diode laser is small and compact and the laser oscillator itself could form part of a mobile rig constructed for this application.

Fig. 1 Concrete slab cut at 1.0–1.2 kW cm^-2 and 2 mm/s with mechanical removal of solidified dross between passes: (a) using a CO2 laser and 94 passes; (b) using a diode laser and 74 passes; and (c) showing the depth dependence of kerf width.

Fig. 2 Calculated and experimental kerf profiles for diode and CO2 lasers after dross removal, after (a) a single laser pass, and (b) after three successive laser beam passes. Crosses indicate experimental data points.

1. Laser cutting for thick concrete by multi-pass technique

Multi-pass 기술에 의한 두꺼운 콘크리트 레이저 절단

Shigeki Muto, Kazuyoku Tei, and Tomoo Fujioka


https://www.osapublishing.org/col/abstract.cfm?uri=col-5-S1-S39

     This paper performed the measurements of attenuation constant of a multi-mode fiber laser. The experiments were conducted using a 5-kW fiber laser (IPG, YLR-5000) with a 1070nm wavelength. The concrete blocks of 400 x 300 x 100 mm3 were used as work pieces. In addition, the experimental variables were laser power, laser speed, core diameter and fiber length. The observed attenuation constant was below 0.7dB/km. This paper demonstrated that 10kW power delivery was feasible through a 250m long fiber with the core diameter of 150 um. The demonstrated concrete cutting technique is a multi-scan technique which includes fiber laser exposure and dross removal in each scan. This technique can be extended to thick concrete slabs more than 1 m without increasing laser power. This technique has the operation time of 1m2 cutting which is as short as the most commonly used techniques. The operation time for 1m2 area cutting with 5kW laser power was estimated within the range of 2-6 hours.

Fig. 1 Schematic of concrete cutting experiment.

Fig. 2 Optical power transmission through a 1-km fiber with

the core diameter of 300 μm.

Table. 1 Operation Time (for 1-m^2 Cutting) and Removal Rate Predicted from Single Scanning at 4 kW

Fig.3 Kerf depth as a function of scanning speed with 4-kW

laser output.

Fig.4 Predicted operation time and scanning number for

1m cutting depth.