Lab Facilities
Selected Facilities
Bruker FTIR spectrometer, Vertex 70 with DTGLS and MCT detector, and rapid scan capabilities
Harrick Scientific diffuse reflectance accessory and microreactor for continuous in situ and operando gas-solid reactions
Pike Technologies low-pressure flow and high temperature ATR microreactor for continuous in situ and operando gas-solid and gas-liquid-solid reactions
Pike Technologies high-pressure in situ cylindrical ATR reactor (Jet Stream) for gas-liquid-solid reactions (up to 1500 psi and 200 oC).
In Situ Research Instruments (ISRI) transmission mode in situ FTIR microreactor
In-house made in situ low void volume reaction cell with for UV-visible, FTIR, or Raman spectroscopies
StellarNet UV-visible miniature spectrometer
Avantes (<200 C), StellarNet (<150 C), Ocean Optics (<80 C) diffuse optical fiber probes
Ocean Optics UV-visible immersion probe
Bruker Raman Senterra spectrometer
In-house made portable gas delivery and control system (with Omega and Brooks mass flow controllers and digital readout box) for in situ reaction units
New Era Pump Systems high pressure syringe pumps
In-house made fixed bed reactor with gas delivery system and online gas sampling and analysis via SRI Instruments gas chromatograph
Thermo Scientific SR3000 Ultimate HPLC system (gradient pump, TCC-300RS column thermostat, DAD-300RS detector, Refractomax 521 detector, and WPS-3000TSL autosampler)
Pfeiffer quadrupole mass spectrometer (OmniStar GSD 301-O3)
CEBC Shared Facilities
Selected Facilities
Parr Instrument Co. stirred pressure reactors provided with HPLC pumps and mass flow controllers, on-line GC and off-line HPLCs
Parr Instrument Co. multiple high-pressure reactors (MOC- Hastelloy C-276 and Ti)
Parr Instrument Co. high-pressure, high-temperature, large volume fixed-bed/trickle-bed reactor
Mettler Toledo ReactIR reaction system equipped with ATR-IR probes at high pressures (<300 bar).
Ocean Optics UV-visible spectrophotometer
Bruker Tensor 27 FTIR spectrometer
Pike Technologies diffuse reflectance DiffusIR accessory
Micromeritics temperature programmed analysis unit (Autochem 2910) for TPR, TPD, TPO and chemisorption
Quantachrome Instruments surface area and pore size analyzer (Nova 2200e)
ICP-OES spectrometer (down to ppb) of various elements (Rh, P, Si) in liquid samples
GC/Mass Spectrometer, GCs, HPLCs
PANalytical Zetium XRF spectrometer
PANalytical Zetium XRD diffractometer