High Priority Objectives:
Automate up to 10 columns within 20 minutes
Each wash consitently uses ~1 mL (± 0.2 mL)
Fluids must be fully purged between washes
Access to columns between washes for manual contribution to the process
Chemical resistance for all distinct solutions (Water, 0.1 N HCl, 1 M NaPO4)
Secondary Priority Objectives:
Insertable tray with slots for filter paper underneath each column to collect samples (properly spaced)
Resin in the column remains visible through each wash
Container beneath columns for disposal of run-through fluid
Separated stages of automation, selectable to resume the process after stopping for manual insertion
Final Design Solution: Fluid Distribution
Reservoirs for each fluid solution
3 Peristaltic pumps to drive fluid flow and 1 air pump
3 Fully primed manifolds for each fluid solution ( 1 inlet to 10 outlets)
Check valves at the end of every outlet before a coming together at the column
Combiner uniting 1 outlet of every manifold and air into a single new outlet (4 inlets to 1 column outlet)
Manual end plugs to stop flow when fewer than 10 columns are being washed, along with electronic selection
Final Design Solution: Control Interface
Main Power Switch (On/Off)
4 Momentary Push Buttons (Manual Priming for Individual Fluids and Air)
2 7-Segment Displays (Process Time + Column Selected/Process Label)
3 Push Buttons (Start, Stop, and Reset)
1 Push Buttons (Looped +1 Column Selection)
Final Design Solution: Component Packaging
3 Pump Mounting on Bottom Base Plate
3 Manifold Mounts (Outlets facing up)
Tiered Perforated Tray (To support tubing upright)
Tiered Tube Rack (To hold tubes at the same height)
Column Holder Tray (Slip fit for columns to be held during the process)
Filter Paper Tray (Used to collect final wash sample)
Microcontroller and PCB Space (Fluid-resistant enclosed area)
Button Control Board (User display and controls)
Final Packaging Overview:
Project Performance Results (Final Prototype)