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Chemoselectivity

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Introduction
Reaction
Purification
Analysis
Clean Up
Conclusion

Chemoselectivity

Home
Introduction
Reaction
Purification
Analysis
Clean Up
Conclusion
More

reaction

After 50 minutes of heating and stirring, you obtain the results below.

video begins with a small long neck round bottom flask containing a small amount of dark brown solution elevated slightly above the surface of a sandbath; the solution appears to be moving slightly, implying stirring; the flask is attached to a distillation head via a rubber connector on a metal rod; one arm of the distillation head is capped with a septum, the other has a thin Teflon tube inserted into its septum; a metal temperature probe with one end in the sand is also visible

photo shows two TLC plates on a lab bench next to a clear plastic ruler whose 0 cm marking is aligned with the origins of the TLC plate; the three lanes on the left TLC plate are labeled, from left to right: “SM,” “t=0,” and “t=10;” the three lanes of the right TLC plate are labeled, from left to right: “20,” “30,” “40,” and “50;” the “SM” lane shows a single pencil circle aligned with the 3.3 cm marking on the ruler; the “t=0,” t=10,” “20,” and “30” lanes show two pencil circles each, one aligned with the 3.3 cm marking and the other approximately alined with the 2.4 cm marking; the “40” and “50” lanes show a single pencil circle, aligned with the lower circle on the other lanes

Isolate the final product!

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