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Rowlands was also in a band called Ariel prior to meeting up with Simons.[3] He formed Ariel in London with friends Brendan Melck and Mathew Berry. Their first single was "Sea of Beats", which was essentially a white label. Before Philip Brown set up Echo Logik Records, their first promo was "Bokadilo". Other songs, released on 12-inch, included "Mustn't Grumble" and their best-known, "Rollercoaster".[3] After a year on Echo Logik they signed to the record label deConstruction. They insisted on a female singer and they recruited former Xpansions frontwoman Sally Ann Marsh, and after some disappointing songs such as "Let It Slide" (Rowlands would later describe it as "a stinker"), the band fell apart. One of the last things Ariel did was the song "T Baby", which was remixed by the pair.

Rowlands and Simons started to DJ at a club called Naked Under Leather in the back of a pub in 1992,which was called the swinging sporran, and then retro bar, Currently still operating under the retro bar name and run by the university of Manchester [3] under the alias, the 237 Turbo Nutters[8] (named after the number of their house on Dickenson Road in Manchester and a reference to their Blackburn raving days). The pair would play hip hop, techno, and house.[10] The two called themselves the Dust Brothers[3] after the US production duo, famous for their work with the Beastie Boys. After a while, Rowlands and Simons began to run out of suitable instrumental hip hop tracks to use, so they started to make their own. Using a Hitachi hi-fi system, an Atari ST, a sampler, and a keyboard, they recorded "Song to the Siren", which sampled This Mortal Coil.[11] "Song to the Siren" was released on their own record label, which they called Diamond Records (after Ed's nickname). At this point the Dust Brothers were the first-ever backroom DJs in the Sumptuous Locarno Lounge at The Job Club in Gossips night club in Dean Street, Soho from April 1992 till April 1993.

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In October 1992, they pressed 500 white-label copies and took them to dance-record shops around London, but all refused to play it, saying it was too slow (the track played at 111 BPM). They sent a copy to London DJ Andrew Weatherall, who made it a permanent fixture in his DJ sets. In May 1993 Steven Hall signed the duo and Junior Boy's Own released "Song to the Siren".[3]

Around June 1993, the Dust Brothers recorded their first remixes. The first was "Packet of Peace" for Justin Robertson's Lionrock group, followed by songs from Leftfield, Republica, and the Sandals. Later in 1993, Rowlands and Simons completed work on their Fourteenth Century Sky EP, released in January 1994.[3] It contained the groundbreaking "Chemical Beats", which epitomised the duo's genre-defining big beat sound.[3] The EP also contained "One Too Many Mornings", which for the first time showed their less intense, more chilled-out side. Both "One Too Many Mornings" and "Chemical Beats" would later appear on their debut album. Fourteenth Century Sky was followed later in 1994 by the My Mercury Mouth EP.[3] "Chemical Beats" was also part of the soundtrack for the first edition of the Wipeout video game series, having been featured in Wipeout for the PlayStation in 1995.

During the 1995 Glastonbury Festival, Noel Gallagher had told them how much he liked Exit Planet Dust, and asked if he could sing on a future track, similar to the way Tim Burgess had worked on "Life Is Sweet". They did not think much of the offer at the time, given how busy Gallagher would be with the release of Oasis' (What's the Story) Morning Glory?, plus the complexities of dealing with each other's record companies. However, the duo later worked on a track they thought would benefit from a vocal. They sent Gallagher a tape of what they had done so far. He worked on it overnight, and left a message early next morning that he was ready to record it. The track was called "Setting Sun" and was finally released in October 1996. It entered the UK chart at the top, giving the duo their first ever No. 1 single.[3] "Setting Sun" was backed by a longer instrumental version, and also a new track "Buzz Tracks", which was not much more than a DJ tool. The three remaining members of the Beatles' lawyers later wrote to the Chemical Brothers, mistakenly claiming they had sampled "Tomorrow Never Knows". Virgin Records hired a musicologist to prove they did not sample the song.

On 7 April 1997, the Chemical Brothers released their second album, Dig Your Own Hole. It was recorded at the band's own south London studio, with the title taken from graffiti on the wall outside. The album was well received,[15] with Mixmag rating it 10/10 and calling it "mad enough to be thrilling, slick enough for not even remotely trendy coffee tables".

At the end of the year, Dig Your Own Hole's final track, the nine-minute-long "The Private Psychedelic Reel", gave rise to a limited-edition mini-EP of the same name. The B-side consisted of a live version of "Setting Sun", recorded at the Lowlands Festival, Netherlands on 24 August 1997. Also in December, following four sold-out US shows, the Chemical Brothers toured the UK, concluding in a sold-out show at Brixton Academy, London.

The "Electronic Battle Weapon" series of promo releases have typically been newly recorded Chemical Brothers tracks, released on promo to allow DJs to test them in a club environment, and to gauge their popularity.

Simons returned to live performances in 2016, performing at the Parklife Festival in Manchester, which included a new setlist and a cover of New Order's "Temptation" with Sumner's recorded vocals.[52] In November 2016, the duo released the non-album single "C-H-E-M-I-C-A-L", which premiered on BBC Radio 1.[53] The song originally debuted as a demo in 2012, created to open the duo's DJ sets from 2012 to 2015.[54]

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