Figure 1(b) shows the X-ray diffraction pattern for as-quenched melt-spun Bi-8.1 at% Zn eutectic alloy. All the peaks were identified for Bi rhombohedral structure. No precipitation of Zn was observed and the structure is a single phase Bi rich solid solution of Zn in Bi. Therefore rapid solidification by melt spinning technique extended the solubility of Zn in Bi up to the eutectic composition. The lattice parameter a is increased and c is decreased and this led to the decrease in the axial ratio c/a (see Table 1). The volume of the unit cell v is increased from 212.298 to 212.608 3. The intensity ratio from (110) plane to (012) plane was decreased from 29% to 6.74%. The particle size was calculated to be 330.7 . The detail of XRD is shown in Table 1.
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