Rigaku XtaLAB mini Benchtop Single Crystal X-Ray Diffraction (Statesboro Campus) (AMCRL03)
Located in room SNR 2223.
Below the specifications is the calendar to schedule appointments, and below that is the calendar showing all already scheduled reservations:
You must be logged into a @georgiasouthern.edu or Gmail account to reserve instrument time.
Charges: $10/sample - full run, External users $50/sample
(Future charges subject to change)
The Rigaku XtaLAB mini II, especially when equipped with a cryo-cooling system, is primarily designed for single crystal X-ray diffraction (SC-XRD) of small molecules. The cryo-cooling option allows for the collection of data at low temperatures.
Here's a breakdown of the samples and capabilities:
Sample Types:
Small Molecule Single Crystals: The XtaLAB mini II is specifically designed to work with small molecule single crystals to determine their 3D structures.
Organic Materials: When equipped with a cryo-cooling stage, it can be used to investigate organic materials, particularly at low 2θ angles.
Capabilities:
Single Crystal Structure Determination: It can determine the 3D structures of small molecules to a publication-quality standard.
Benchtop Operation: Its compact size allows it to be placed on a standard lab bench, making it accessible to individual research groups.
Low-Temperature Data Collection: The optional cryo-cooling system (e.g., Oxford Cryostream 800) enables data collection at low temperatures, which can be useful for studying temperature-sensitive materials or improving data quality.
User-Friendly Software: It comes with CrysAlisPro software for data collection and processing, with automated features like crystal screening and structure solution.
Reduced Size, Undiminished Quality: Despite its compact size, the XtaLAB mini II maintains research-grade data quality for accurate structural determination.
"What is this?" Feature: This feature allows for rapid sample identification before committing to a full data collection.
In essence, the XtaLAB mini II with cryo-cooling is a valuable tool for chemists and material scientists who need to determine the structures of their synthesized compounds or investigate the behavior of materials at low temperatures. The optional cryo-cooling system expands its utility for studies involving temperature-dependent phenomena or working with crystals that diffract weakly at room temperature.
User document(s) for Single Crystal XRD Software:
1 - CrysAlis Pro (CAP) Quick User Guide
2 - CrysAlis Pro (CAP) Procedures for creating a crystal movie and absorption correction model.
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