Part II

Add the Part I crude product, a stir bar, and 2 mL of 3M HCl to the reaction flask.

transfer Part I crude

photo shows a metal spatula inserted into the neck of a small round bottom flask; there is a small clump of gray putty on the end of the spatula that is about to drop into the bottom of the flask

measure out HCl

photo shows a graduated reaction tube with a clear liquid filled up to the 2.0 mL marking; next to the tube is a translucent plastic reagent bottle labeled “3 M HCl”

add HCl to reaction apparatus

video shows a small round bottom flask with a small amount of golden solution and a magnetic stir bar nestled into a sandbath; the roundbottom flask is fitted with a condenser via a connector attached to a metal bar, which is in turn attached to a distillation head via a rubber adaptor; a graduated test tube partially filled with clear liquid is visible, as is a glass pipette, the latter of which is used to dispense some of the clear liquid into the round bottom flask via the vertical arm of the distillation head; a second portion of clear liquid is pipetted from the graduated test tube into the round bottom flask

Start the reaction!

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