Search this site

Embedded Files

Synthesis of Carboline

Home
Introduction
Part I
Part II
Part III
Analysis
Clean Up
Conclusion

Synthesis of Carboline

Home
Introduction
Part I
Part II
Part III
Analysis
Clean Up
Conclusion
More

Part I

Filter your reaction mixture of a Hirsch funnel and wash three times with distilled water.

video shows a yellowish slurry being poured out of a small Erlenmeyer flask into a plastic Hirsch funnel attached a filter flask; the filter flask is fitted into one of the plastic tubes of a three-way vacuum valve; liquid trickles through the funnel while off-white solids remain caught in the funnel; a graduated cylinder with a small portion of water then appears and a glass pipette is used to drizzle three 1 mL portions over the solids caught in the funnel

photo shows a Hirsch funnel fitted into a small glass filter flask with a rubber adapter; the filter flask is attached to a plastic hose leading off camera; a caking of dried, off-white solid is visible in the Hirsch funnel, along with a magnetic stirrer; yellow liquid is visible in the bottom of the filter flask

Weigh the crude product.

© UC Berkeley

Report abuse

Page details

Page updated

Report abuse